2-(4-CHLOROPHENYL)-5'-FLUORO-2'-HYDROXYACETOPHENONE

Base Information

• Chemical Name: 2-(4-CHLOROPHENYL)-5'-FLUORO-2'-HYDROXYACETOPHENONE
• CAS No.: 527751-48-0
• Molecular Formula: C₁₄H₁₀ClFO₂
• Molecular Weight: 264.684
• Hs Code.: 2914790090
• Mol file: 527751-48-0.mol

Synonyms:2-(4-chlorophenyl)-1-(5-fluoro-2-hydroxyphenyl)ethanone

Chemical Property of 2-(4-CHLOROPHENYL)-5'-FLUORO-2'-HYDROXYACETOPHENONE

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

2-(4-Chlorophenyl)-1-(5-fluoro-2-hydroxyphenyl)ethanone 97% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of 2-(4-CHLOROPHENYL)-5'-FLUORO-2'-HYDROXYACETOPHENONE

There total 3 articles about 2-(4-CHLOROPHENYL)-5'-FLUORO-2'-HYDROXYACETOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

(4-Chloro-phenyl)-acetic acid 4-fluoro-phenyl ester (183280-14-0) → 2-(4-chlorophenyl)-1-(5-fluoro-2-hydroxyphenyl)ethanone (527751-48-0)

Guidance literature:

With aluminium trichloride; at 150 - 180 ℃;

Reference yield:

4-Fluorophenol (371-41-5) → 2-(4-chlorophenyl)-1-(5-fluoro-2-hydroxyphenyl)ethanone (527751-48-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / Et₃N / diethyl ether / 1 h / Heating

2: 32 percent / AlCl₃ / 150 - 180 °C

With aluminium trichloride; triethylamine; In diethyl ether;

Reference yield:

4-chlorophenacetyl chloride (25026-34-0) → 2-(4-chlorophenyl)-1-(5-fluoro-2-hydroxyphenyl)ethanone (527751-48-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / Et₃N / diethyl ether / 1 h / Heating

2: 32 percent / AlCl₃ / 150 - 180 °C

With aluminium trichloride; triethylamine; In diethyl ether;

upstream raw materials:

(4-Chloro-phenyl)-acetic acid 4-fluoro-phenyl ester

4-Fluorophenol

4-chlorophenacetyl chloride

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