(2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(((benzyloxy)carbonyl)amino)ethoxy) tetrahydro-2H-pyran-3,4,5-triyl triacetate

Base Information

Chemical Name:(2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(((benzyloxy)carbonyl)amino)ethoxy) tetrahydro-2H-pyran-3,4,5-triyl triacetate
CAS No.:153253-02-2
Molecular Formula:C₂₄H₃₁NO₁₂
Molecular Weight:525.51
Hs Code.:

Synonyms:(2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(((benzyloxy)carbonyl)amino)ethoxy) tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Chemical Property of (2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(((benzyloxy)carbonyl)amino)ethoxy) tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Technology Process of (2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(((benzyloxy)carbonyl)amino)ethoxy) tetrahydro-2H-pyran-3,4,5-triyl triacetate

There total 10 articles about (2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(((benzyloxy)carbonyl)amino)ethoxy) tetrahydro-2H-pyran-3,4,5-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 77987-49-6
benzyl 2-hydroxyethylcarbamate

: 86520-63-0
2,3,4,6-tetra-O-acetyl-α-galactopyranosyl trichloroacetimidate

: 153253-02-2
(2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(((benzyloxy)carbonyl)amino)ethoxy) tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; toluene; at 0 ℃; for 0.5h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2012.03.039

Reference yield: 63.0%

: 77987-49-6
benzyl 2-hydroxyethylcarbamate

: 3068-32-4
1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

: 153253-02-2
(2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(((benzyloxy)carbonyl)amino)ethoxy) tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: With mercury(II) cyanide; In acetonitrile; at 20 ℃; for 24h;
DOI:10.1039/b513944a

Reference yield: 62.0%

: 77987-49-6
benzyl 2-hydroxyethylcarbamate

: 4163-60-4
β-D-galactose peracetate

: 153253-02-2
(2R,3S,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(((benzyloxy)carbonyl)amino)ethoxy) tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 2-(benzyloxycarbonyl)aminoethyl 2,3,4,6-tetra-O-acetyl-α-D-galactopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In acetonitrile; at 0 - 20 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.3762/bjoc.6.81