1-(1',4-dimethyl-1-phenyl-1H,1'H-[3,4'-bipyrazol]-5-yl)-3-(1-phenyl-3-(2,2,2-trifluoroethyl)-1H-pyrazol-5-yl)urea

Base Information

Chemical Name:1-(1',4-dimethyl-1-phenyl-1H,1'H-[3,4'-bipyrazol]-5-yl)-3-(1-phenyl-3-(2,2,2-trifluoroethyl)-1H-pyrazol-5-yl)urea
CAS No.:1610051-02-9
Molecular Formula:C₂₆H₂₃F₃N₈O
Molecular Weight:520.517
Hs Code.:

Synonyms:1-(1',4-dimethyl-1-phenyl-1H,1'H-[3,4'-bipyrazol]-5-yl)-3-(1-phenyl-3-(2,2,2-trifluoroethyl)-1H-pyrazol-5-yl)urea

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Chemical Property of 1-(1',4-dimethyl-1-phenyl-1H,1'H-[3,4'-bipyrazol]-5-yl)-3-(1-phenyl-3-(2,2,2-trifluoroethyl)-1H-pyrazol-5-yl)urea

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Technology Process of 1-(1',4-dimethyl-1-phenyl-1H,1'H-[3,4'-bipyrazol]-5-yl)-3-(1-phenyl-3-(2,2,2-trifluoroethyl)-1H-pyrazol-5-yl)urea

There total 4 articles about 1-(1',4-dimethyl-1-phenyl-1H,1'H-[3,4'-bipyrazol]-5-yl)-3-(1-phenyl-3-(2,2,2-trifluoroethyl)-1H-pyrazol-5-yl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1414571-74-6
phenyl (1‘,4-dimethyl-1-phenyl-1H,1‘H-[3,4’-bipyrazol]-5-yl)carbamate

: C₁₁H₁₀F₃N₃

: 1610051-02-9
1-(1',4-dimethyl-1-phenyl-1H,1'H-[3,4'-bipyrazol]-5-yl)-3-(1-phenyl-3-(2,2,2-trifluoroethyl)-1H-pyrazol-5-yl)urea

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 14h;

Reference yield:

: 85290-80-8
ethyl 1-methylpyrazole-4-carboxylate

: 1610051-02-9
1-(1',4-dimethyl-1-phenyl-1H,1'H-[3,4'-bipyrazol]-5-yl)-3-(1-phenyl-3-(2,2,2-trifluoroethyl)-1H-pyrazol-5-yl)urea

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1.5 h / -80 - -79 °C / Inert atmosphere

1.2: -76 - 20 °C

2.1: ethanol / 20 °C / Reflux

3.1: sodium hydroxide / ethyl acetate / 2.5 h / 20 °C

4.1: triethylamine / dichloromethane / 14 h / 20 °C

With triethylamine; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;

Reference yield:

: 1414571-72-4
2-methyl-3-(1-methyl-1H-pyrazol-4-yl)-3-oxopropanenitrile

: 1610051-02-9
1-(1',4-dimethyl-1-phenyl-1H,1'H-[3,4'-bipyrazol]-5-yl)-3-(1-phenyl-3-(2,2,2-trifluoroethyl)-1H-pyrazol-5-yl)urea

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 20 °C / Reflux

2: sodium hydroxide / ethyl acetate / 2.5 h / 20 °C

3: triethylamine / dichloromethane / 14 h / 20 °C

With triethylamine; sodium hydroxide; In ethanol; dichloromethane; ethyl acetate;