cis-1a-(4-(4-chlorophenyl)cyclohexyl)naphtho[2,3-b]oxirene-2,7(1aH,7aH)dione

Base Information

Chemical Name:cis-1a-(4-(4-chlorophenyl)cyclohexyl)naphtho[2,3-b]oxirene-2,7(1aH,7aH)dione
CAS No.:1409957-42-1
Molecular Formula:C₂₂H₁₉ClO₃
Molecular Weight:366.844
Hs Code.:

Synonyms:cis-1a-(4-(4-chlorophenyl)cyclohexyl)naphtho[2,3-b]oxirene-2,7(1aH,7aH)dione

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Chemical Property of cis-1a-(4-(4-chlorophenyl)cyclohexyl)naphtho[2,3-b]oxirene-2,7(1aH,7aH)dione

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Technology Process of cis-1a-(4-(4-chlorophenyl)cyclohexyl)naphtho[2,3-b]oxirene-2,7(1aH,7aH)dione

There total 3 articles about cis-1a-(4-(4-chlorophenyl)cyclohexyl)naphtho[2,3-b]oxirene-2,7(1aH,7aH)dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1203609-10-2
cis-2-[4-(4-chlorophenyl)cyclohexyl]-1,4-naphthoquinone

: 1409957-42-1
cis-1a-(4-(4-chlorophenyl)cyclohexyl)naphtho[2,3-b]oxirene-2,7(1aH,7aH)dione

Guidance literature:: With dihydrogen peroxide; sodium carbonate; In 1,4-dioxane; at 80 ℃; for 0.5h;

Reference yield:

: 1409956-99-5
cis/trans-2-(4-(4-chlorophenyl)cyclohexyl)naphthalen-1-ol

: 1409957-42-1
cis-1a-(4-(4-chlorophenyl)cyclohexyl)naphtho[2,3-b]oxirene-2,7(1aH,7aH)dione

Guidance literature:: Multi-step reaction with 3 steps

1: cyclohexane / 1 h / Resolution of racemate

2: sodium nitrite; sulfuric acid / 1,4-dioxane; water / 2 h / 5 - 80 °C

3: sodium carbonate; dihydrogen peroxide / 1,4-dioxane / 0.5 h / 80 °C

With sulfuric acid; dihydrogen peroxide; sodium carbonate; sodium nitrite; In 1,4-dioxane; cyclohexane; water;

Reference yield:

: 1409957-10-3
cis-2-(4-(4-chlorophenyl)cyclohexyl)naphthalen-1-ol

: 1409957-42-1
cis-1a-(4-(4-chlorophenyl)cyclohexyl)naphtho[2,3-b]oxirene-2,7(1aH,7aH)dione

Guidance literature:: Multi-step reaction with 2 steps

1: sodium nitrite; sulfuric acid / 1,4-dioxane; water / 2 h / 5 - 80 °C

2: sodium carbonate; dihydrogen peroxide / 1,4-dioxane / 0.5 h / 80 °C

With sulfuric acid; dihydrogen peroxide; sodium carbonate; sodium nitrite; In 1,4-dioxane; water;