bis(benzoyloxymethyl)zinc

Base Information

• Chemical Name: bis(benzoyloxymethyl)zinc
• CAS No.: 15614-71-8
• Molecular Formula: C₁₆H₁₄O₄Zn
• Molecular Weight: 335.675
• Mol file: 15614-71-8.mol

Synonyms:bis(benzoyloxymethyl)zinc

Chemical Property of bis(benzoyloxymethyl)zinc

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(benzoyloxymethyl)zinc

There total 2 articles about bis(benzoyloxymethyl)zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

iodomethylbenzoate (13943-33-4) + diethylzinc (557-20-0) → bis(benzoyloxymethyl)zinc (15614-71-8)

Guidance literature:

In dichloromethane-d2; Irradiation (UV/VIS); irradiation of Et2Zn (0.5 equiv.) and PhCO2CH2I in CD2Cl2;

DOI:10.1021/ja0109287

Reference yield: 43.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + zinc benzoate (553-72-0) → bis(benzoyloxymethyl)zinc (15614-71-8)

Guidance literature:

In diethyl ether; Zn compound treated with CH2N2 (3 equiv.) in Et2O;

DOI:10.1021/ja0109287

upstream raw materials:

iodomethylbenzoate

diethylzinc

diazomethane

zinc benzoate