C₂₃H₂₀N₆O₂S

Base Information

Chemical Name:C₂₃H₂₀N₆O₂S
CAS No.:1260105-64-3
Molecular Formula:C₂₃H₂₀N₆O₂S
Molecular Weight:444.517
Hs Code.:

C<sub>23</sub>H<sub>20</sub>N<sub>6</sub>O<sub>2</sub>S

Synonyms:C₂₃H₂₀N₆O₂S

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Chemical Property of C₂₃H₂₀N₆O₂S

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Technology Process of C₂₃H₂₀N₆O₂S

There total 13 articles about C₂₃H₂₀N₆O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₁N₅O₃S

: 1260105-64-3
C₂₃H₂₀N₆O₂S

Guidance literature:: With hydrazine hydrate; In 1-methyl-pyrrolidin-2-one; at 100 - 200 ℃; for 1.5h; Microwave irradiation;

Reference yield:

: 89489-53-2
tetrahydro-2H-thiopyran-4-carboxylic acid

: 1260105-64-3
C₂₃H₂₀N₆O₂S

Guidance literature:: Multi-step reaction with 13 steps

1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 20 °C

1.2: 4.5 h / -78 - 20 °C

2.1: toluene / 18 h / 110 °C / Inert atmosphere

3.1: trichlorophosphate; N,N-dimethyl-aniline / 5 h / 50 °C

4.1: ammonia / methanol / 5 h / 80 °C / Sealed tube

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 50 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; Oxone / water; methanol / 6 h / 20 °C

7.1: N-iodo-succinimide / acetonitrile / 1 h / 20 °C

8.1: potassium phosphate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 90 °C / Inert atmosphere

9.1: N-Bromosuccinimide / acetonitrile / 2 h / 20 °C

10.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 1 h / 150 °C / Microwave irradiation

11.1: osmium(VIII) oxide; 2,6-dimethylpyridine; water / 1,4-dioxane / 0.33 h / 20 °C

11.2: 96 h / 20 °C

12.1: trifluoroacetic acid; water

13.1: hydrazine hydrate / 1-methyl-pyrrolidin-2-one / 1.5 h / 100 - 200 °C / Microwave irradiation

With 2,6-dimethylpyridine; Oxone; potassium phosphate; N-Bromosuccinimide; N-iodo-succinimide; osmium(VIII) oxide; ammonia; water; sodium hydrogencarbonate; hydrazine hydrate; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; trifluoroacetic acid; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; water; toluene; acetonitrile; 10.1: Stille Coupling;

Reference yield:

: 1260105-87-0
7-chloro-5-(tetrahydro-2H-thiopyran-4-yl)pyrazolo[1,5-a]pyrimidine

: 1260105-64-3
C₂₃H₂₀N₆O₂S

Guidance literature:: Multi-step reaction with 10 steps

1.1: ammonia / methanol / 5 h / 80 °C / Sealed tube

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 50 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; Oxone / water; methanol / 6 h / 20 °C

4.1: N-iodo-succinimide / acetonitrile / 1 h / 20 °C

5.1: potassium phosphate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 90 °C / Inert atmosphere

6.1: N-Bromosuccinimide / acetonitrile / 2 h / 20 °C

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 1 h / 150 °C / Microwave irradiation

8.1: osmium(VIII) oxide; 2,6-dimethylpyridine; water / 1,4-dioxane / 0.33 h / 20 °C

8.2: 96 h / 20 °C

9.1: trifluoroacetic acid; water

10.1: hydrazine hydrate / 1-methyl-pyrrolidin-2-one / 1.5 h / 100 - 200 °C / Microwave irradiation

With 2,6-dimethylpyridine; Oxone; potassium phosphate; N-Bromosuccinimide; N-iodo-succinimide; osmium(VIII) oxide; ammonia; water; sodium hydrogencarbonate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; water; acetonitrile; 7.1: Stille Coupling;