3-Cyan-2-cyclohexyl-3,4,5,6-tetrahydro-6-phenyl-2H-1,2-oxazin-5-carbonsaeure-ethylester

Base Information

Chemical Name:3-Cyan-2-cyclohexyl-3,4,5,6-tetrahydro-6-phenyl-2H-1,2-oxazin-5-carbonsaeure-ethylester
CAS No.:83341-69-9
Molecular Formula:C₂₀H₂₆N₂O₃
Molecular Weight:342.438
Hs Code.:

Synonyms:3-Cyan-2-cyclohexyl-3,4,5,6-tetrahydro-6-phenyl-2H-1,2-oxazin-5-carbonsaeure-ethylester

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Chemical Property of 3-Cyan-2-cyclohexyl-3,4,5,6-tetrahydro-6-phenyl-2H-1,2-oxazin-5-carbonsaeure-ethylester

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Technology Process of 3-Cyan-2-cyclohexyl-3,4,5,6-tetrahydro-6-phenyl-2H-1,2-oxazin-5-carbonsaeure-ethylester

There total 3 articles about 3-Cyan-2-cyclohexyl-3,4,5,6-tetrahydro-6-phenyl-2H-1,2-oxazin-5-carbonsaeure-ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37898-41-2
N-(2-Chlorethyliden)cyclohexylamin-N-oxid

: 151-50-8
potassium cyanide

: 4192-77-2
ethyl cinnamate

: 140-10-3
(E)-3-phenylacrylic acid

: 83341-69-9
3-Cyan-2-cyclohexyl-3,4,5,6-tetrahydro-6-phenyl-2H-1,2-oxazin-5-carbonsaeure-ethylester

Guidance literature:: With silver tetrafluoroborate; Yield given. Multistep reaction. Yields of byproduct given; 1) lig. SO₂/1,2-dichloroethane, -10 deg C, 1 h, 2) 1,2-dichloroethane/H₂O, 5 min;

Reference yield:

: 37898-41-2
N-(2-Chlorethyliden)cyclohexylamin-N-oxid

: 83341-69-9
3-Cyan-2-cyclohexyl-3,4,5,6-tetrahydro-6-phenyl-2H-1,2-oxazin-5-carbonsaeure-ethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) AgBF₄ / 1) 1,2-dichloroethane, 0 deg C, 1 h, 2) 1,2-dichloroethane/water, 5 min

2: 1) AgBF₄ / 1) lig. SO₂/1,2-dichloroethane, -10 deg C, 1 h, 2) 1,2-dichloroethane/H₂O, 5 min

With silver tetrafluoroborate;

Reference yield:

: 37898-41-2
N-(2-Chlorethyliden)cyclohexylamin-N-oxid

: 151-50-8
potassium cyanide

: 83341-69-9
3-Cyan-2-cyclohexyl-3,4,5,6-tetrahydro-6-phenyl-2H-1,2-oxazin-5-carbonsaeure-ethylester

: 4192-77-2
ethyl cinnamate

Guidance literature:: With silver tetrafluoroborate; Yield given. Multistep reaction. Yields of byproduct given; 1) 1,2-dichloroethane, 0 deg C, 1 h, 2) 1,2-dichloroethane/water, 5 min;