zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO₂C₂(CH₃)4)-meso-porphyrin

Base Information

Chemical Name:zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO₂C₂(CH₃)4)-meso-porphyrin
CAS No.:1110667-97-4
Molecular Formula:C₆₀H₆₇BN₄O₂Zn
Molecular Weight:952.419
Hs Code.:

zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO<sub>2</sub>C<sub>2</sub>(CH<sub>3</sub>)4)-meso-porphyrin

Synonyms:zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO₂C₂(CH₃)4)-meso-porphyrin

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Chemical Property of zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO₂C₂(CH₃)4)-meso-porphyrin

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Technology Process of zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO₂C₂(CH₃)4)-meso-porphyrin

There total 1 articles about zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO₂C₂(CH₃)4)-meso-porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1000867-39-9
zinc(II)-5,15-bis-(3,5-di-tertbutylphenyl)-10-phenyl-20-iodoporphyrin

: 5970-45-6
zinc(II) acetate dihydrate

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1110667-97-4
zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO₂C₂(CH₃)4)-meso-porphyrin

Guidance literature:: zinc(II)-5,15-bis-(3,5-di-tertbutylphenyl)-10-phenyl-20-iodoporphyrin; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In 1,2-dichloro-ethane; at 90 ℃; for 15h; Inert atmosphere;

zinc(II) acetate dihydrate; In methanol; dichloromethane; at 20 ℃;
DOI:10.1039/d0tc03490h

Reference yield: 80.0%

: 1110667-97-4
zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO₂C₂(CH₃)4)-meso-porphyrin

: 16294-34-1
1,8-dimethoxyanthracene

: 1060286-04-5
[5,6-[4,10-(1,8-dimethoxyanthracene)]-10,20-bis-(3,5-di-tert-butylphenyl)-15-phenylporphyrinato]zinc(II)

Guidance literature:: 1,8-dimethoxyanthracene; With pyridine; N-Bromosuccinimide; In chloroform; at 60 ℃; for 3h;

zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO₂C₂(CH₃)4)-meso-porphyrin; With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium hydroxide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In m-xylene; at 90 ℃; for 72h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; scandium tris(trifluoromethanesulfonate); In dichloromethane; at 40 ℃; Inert atmosphere;
DOI:10.1021/ol801500b

Reference yield: 70.0%

: 1110667-97-4
zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(BO₂C₂(CH₃)4)-meso-porphyrin

: 34244-15-0
1-iodopyrene

: 664310-31-0
zinc(II) (phenyl)(3,5-di-tert-butylphenyl)2(pyrenyl)-meso-porphyrin

Guidance literature:: With barium dihydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; Suzuki-Miyaura coupling reaction;
DOI:10.1246/cl.2004.40