((C₆H₅)3P)2PtCH₂C(NHC₆H₄NO₂)CHC₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=[((C₆H₅)3P)2Pt(CH₂C(NHC₆H₄NO₂)CHC₆H₅)](CF₃SO₃)

Base Information

• Chemical Name: ((C₆H₅)3P)2PtCH₂C(NHC₆H₄NO₂)CHC₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=[((C₆H₅)3P)2Pt(CH₂C(NHC₆H₄NO₂)CHC₆H₅)](CF₃SO₃)
• CAS No.: 169303-25-7
• Molecular Formula: CF₃O₃S*C₅₁H₄₃N₂O₂P₂Pt
• Molecular Weight: 1122.01

Synonyms:((C₆H₅)3P)2PtCH₂C(NHC₆H₄NO₂)CHC₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=[((C₆H₅)3P)2Pt(CH₂C(NHC₆H₄NO₂)CHC₆H₅)](CF₃SO₃)

Chemical Property of ((C₆H₅)3P)2PtCH₂C(NHC₆H₄NO₂)CHC₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=[((C₆H₅)3P)2Pt(CH₂C(NHC₆H₄NO₂)CHC₆H₅)](CF₃SO₃)

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Technology Process of ((C₆H₅)3P)2PtCH₂C(NHC₆H₄NO₂)CHC₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=[((C₆H₅)3P)2Pt(CH₂C(NHC₆H₄NO₂)CHC₆H₅)](CF₃SO₃)

There total 1 articles about ((C₆H₅)3P)2PtCH₂C(NHC₆H₄NO₂)CHC₆H₅⁽¹⁺⁾*CF₃SO₃^(1-)=[((C₆H₅)3P)2Pt(CH₂C(NHC₆H₄NO₂)CHC₆H₅)](CF₃SO₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

[(PPh3)2Pt(η(3)-CH2CCPh)](CF3SO3) + 4-nitro-aniline (100-01-6,104810-17-5) → ((C6H5)3P)2PtCH2C(NHC6H4NO2)CHC6H5(1+)*CF3SO3(1-)=[((C6H5)3P)2Pt(CH2C(NHC6H4NO2)CHC6H5)](CF3SO3) (169303-25-7)

Guidance literature:

In dichloromethane; stirring for 4 days; removing all volatiles, recrystn. (benzene/pentane), syn/anti mixt., elem. anal.;

DOI:10.1016/0020-1693(94)03983-6

Reference yield: 90.0%

((C6H5)3P)2PtCH2C(NHC6H4NO2)CHC6H5(1+)*CF3SO3(1-)=[((C6H5)3P)2Pt(CH2C(NHC6H4NO2)CHC6H5)](CF3SO3) (169303-25-7) → (P(C6H5)3)2Pt(CH2CN(NO2C6H4)CHC6H5) (158847-41-7,169303-19-9,158932-58-2)

Guidance literature:

With PhLi; In tetrahydrofuran;

DOI:10.1016/0020-1693(94)03983-6

upstream raw materials:

4-nitro-aniline

Downstream raw materials:

(P(C₆H₅)3)2Pt(CH₂CN(NO₂C₆H₄)CHC₆H₅)

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