7-O-benzyl-5-O-hexanoylapigenin-4'-yl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside

Base Information

• Chemical Name: 7-O-benzyl-5-O-hexanoylapigenin-4'-yl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside
• CAS No.: 1145669-53-9
• Molecular Formula: C₅₅H₄₈O₁₃
• Molecular Weight: 916.978
• Mol file: 1145669-53-9.mol

Synonyms:7-O-benzyl-5-O-hexanoylapigenin-4'-yl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside

Chemical Property of 7-O-benzyl-5-O-hexanoylapigenin-4'-yl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 7-O-benzyl-5-O-hexanoylapigenin-4'-yl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside

There total 1 articles about 7-O-benzyl-5-O-hexanoylapigenin-4'-yl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

7-O-benzyl-5-O-hexanoyl apigenin (1145669-52-8) + 2,3,4-O-tribenzoyl-α,β-L-rhamnopyranoside → 7-O-benzyl-5-O-hexanoylapigenin-4'-yl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside (1145669-53-9)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In N,N-dimethyl-formamide; at -20 - 20 ℃; for 8h; Molecular sieve; Inert atmosphere;

DOI:10.1016/j.carres.2008.12.016

Reference yield: 79.0%

7-O-benzyl-5-O-hexanoylapigenin-4'-yl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside (1145669-53-9) → 5-O-hexanoylapigenin-4'-yl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside (1145669-54-0)

Guidance literature:

With formic acid; 10% Pd on charcoal; hydrogen; In ethanol; dichloromethane; at 45 ℃; for 9h; under 760.051 Torr;

DOI:10.1016/j.carres.2008.12.016

upstream raw materials:

7-O-benzyl-5-O-hexanoyl apigenin

Downstream raw materials:

5-O-hexanoylapigenin-4'-yl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside