Technology Process of C12H14O2S
There total 2 articles about C12H14O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Grubbs catalyst first generation;
In
dichloromethane;
optical yield given as %ee;
Reflux;
Inert atmosphere;
DOI:10.1021/ol200197v
- Guidance literature:
-
Multi-step reaction with 3 steps
1: propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-(1-phenyl-ethyl)-amine / dichloromethane / 12 h / 15 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
3: Grubbs catalyst first generation / dichloromethane / Reflux; Inert atmosphere
With
Grubbs catalyst first generation; propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; 3-chloro-benzenecarboperoxoic acid; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-(1-phenyl-ethyl)-amine;
In
dichloromethane;
DOI:10.1021/ol200197v