1⁴-methoxy-8⁴-methylsulfonyl-2²,3³,4²,5³,6²,7³-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl

Base Information

• Chemical Name: 1⁴-methoxy-8⁴-methylsulfonyl-2²,3³,4²,5³,6²,7³-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl
• CAS No.: 406217-67-2
• Molecular Formula: C₈₆H₉₈O₂₁S
• Molecular Weight: 1499.78

Synonyms:1⁴-methoxy-8⁴-methylsulfonyl-2²,3³,4²,5³,6²,7³-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl

Chemical Property of 1⁴-methoxy-8⁴-methylsulfonyl-2²,3³,4²,5³,6²,7³-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl

Chemical Property:

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Technology Process of 1⁴-methoxy-8⁴-methylsulfonyl-2²,3³,4²,5³,6²,7³-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl

There total 1 articles about 1⁴-methoxy-8⁴-methylsulfonyl-2²,3³,4²,5³,6²,7³-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C86H98O19S (406217-65-0) → 14-methoxy-84-methylsulfonyl-22,33,42,53,62,73-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl (406217-67-2)

Guidance literature:

C₈₆H₉₈O₁₉S; With disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.5h;

With potassium permanganate; magnesium sulfate; In acetone; at 0 ℃; for 1h; Further stages.;

DOI:10.1021/ja017497c

Reference yield:

H-Leu-Lys(BOC)-Leu-NH2 + 14-methoxy-84-methylsulfonyl-22,33,42,53,62,73-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl (406217-67-2) → 14-methoxy-84-methylsulfonyl-22,33,42,53,62,73-hexa(metoxycarbonyl-L-leucine-L-lysine-L-leucine-amino)-p-octiphenyl

Guidance literature:

1⁴-methoxy-8⁴-methylsulfonyl-2²,3³,4²,5³,6²,7³-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl; With trifluoroacetic acid; In dichloromethane; for 1.5h;

H-Leu-Lys(BOC)-Leu-NH₂; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h; Further stages.;

DOI:10.1021/ja017497c

Reference yield:

14-methoxy-84-methylsulfonyl-22,33,42,53,62,73-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl (406217-67-2) → C62H50O21S

Guidance literature:

With trifluoroacetic acid;

DOI:10.1021/ja017497c

upstream raw materials:

C₈₆H₉₈O₁₉S

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