ethyl 2-((2-aminoethyl)(benzyloxycarbonyl)amino)acetate hydrochloride

Base Information

Chemical Name:ethyl 2-((2-aminoethyl)(benzyloxycarbonyl)amino)acetate hydrochloride
CAS No.:1413927-61-3
Molecular Formula:C₁₄H₂₀N₂O₄*ClH
Molecular Weight:316.785
Hs Code.:

Synonyms:ethyl 2-((2-aminoethyl)(benzyloxycarbonyl)amino)acetate hydrochloride

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Chemical Property of ethyl 2-((2-aminoethyl)(benzyloxycarbonyl)amino)acetate hydrochloride

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Technology Process of ethyl 2-((2-aminoethyl)(benzyloxycarbonyl)amino)acetate hydrochloride

There total 4 articles about ethyl 2-((2-aminoethyl)(benzyloxycarbonyl)amino)acetate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 72648-81-8
C₁₉H₂₈N₂O₆

: 1413927-61-3
ethyl 2-((2-aminoethyl)(benzyloxycarbonyl)amino)acetate hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

Reference yield:

: ethyl N-(2-(tert-butyloxycarbonylamino)ethyl) glycinate hydrochloride

: 1413927-61-3
ethyl 2-((2-aminoethyl)(benzyloxycarbonyl)amino)acetate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / toluene / 2 h / Inert atmosphere

2: acetyl chloride / ethanol / 1 h / 0 - 20 °C / Inert atmosphere

With triethylamine; acetyl chloride; In ethanol; toluene;
DOI:10.1016/j.tetlet.2012.10.032

Reference yield:

: 72648-80-7
ethyl 2-[2-(tert-butoxycarbonylamino)ethyl-[3-[[4-(4,5-difluoro-2-methylsulfanyl-phenyl)phenoxy]methyl]benzoyl]amino]acetate

: 1413927-61-3
ethyl 2-((2-aminoethyl)(benzyloxycarbonyl)amino)acetate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / diethyl ether / 1 h / 0 °C / Inert atmosphere

2: triethylamine / toluene / 2 h / Inert atmosphere

3: acetyl chloride / ethanol / 1 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; triethylamine; acetyl chloride; In diethyl ether; ethanol; toluene;
DOI:10.1016/j.tetlet.2012.10.032