3,5-bis-<3',3'-dimethylallyl>-coumaric acid acetate

Base Information

• Chemical Name: 3,5-bis-<3',3'-dimethylallyl>-coumaric acid acetate
• CAS No.: 107390-24-9
• Molecular Formula: C₂₁H₂₆O₄
• Molecular Weight: 342.435
• Mol file: 107390-24-9.mol

Synonyms:3,5-bis-<3',3'-dimethylallyl>-coumaric acid acetate

Chemical Property of 3,5-bis-<3',3'-dimethylallyl>-coumaric acid acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-bis-<3',3'-dimethylallyl>-coumaric acid acetate

There total 1 articles about 3,5-bis-<3',3'-dimethylallyl>-coumaric acid acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

acetic anhydride (108-24-7) + artepillin C (72944-19-5,78835-00-4) → 3,5-bis-<3',3'-dimethylallyl>-coumaric acid acetate (107390-24-9)

Guidance literature:

With pyridine; at 20 ℃; for 12h;

DOI:10.1016/j.bmc.2021.116372

Reference yield: 93.0%

N’-Boc-L-tryptophan benzyl ester (1170940-54-1) + 3,5-bis-<3',3'-dimethylallyl>-coumaric acid acetate (107390-24-9) → (E)-N-(3,5-diprenyl-4-acetoxy cinnamoyl)-(N'-Boc-L-tryptophan)benzyl ester

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2021.116372

Reference yield: 87.0%

L-serine benzyl ester (1738-72-3) + 3,5-bis-<3',3'-dimethylallyl>-coumaric acid acetate (107390-24-9) → (E)-N-(3,5-diprenyl-4-acetoxy cinnamoyl)-L-serine benzyl ester

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2021.116372

upstream raw materials:

acetic anhydride

artepillin C

Downstream raw materials:

3-[4-acetoxy-3,5-bis(3-methyl-2-butenyl)phenyl]-(2E)-propenoic acid methyl ester