(2-Mercaptobenzothiazolyl)-(methyl 6-O-tertbutyldiphenylsilyl-2-deoxy-α-D-glucopyranosid-2-yl)-isophthalate

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Chemical Name:(2-Mercaptobenzothiazolyl)-(methyl 6-O-tertbutyldiphenylsilyl-2-deoxy-α-D-glucopyranosid-2-yl)-isophthalate
CAS No.:261967-58-2
Molecular Formula:C₃₈H₃₉NO₈S₂Si
Molecular Weight:729.947
Hs Code.:

Synonyms:(2-Mercaptobenzothiazolyl)-(methyl 6-O-tertbutyldiphenylsilyl-2-deoxy-α-D-glucopyranosid-2-yl)-isophthalate

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Chemical Property of (2-Mercaptobenzothiazolyl)-(methyl 6-O-tertbutyldiphenylsilyl-2-deoxy-α-D-glucopyranosid-2-yl)-isophthalate

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Technology Process of (2-Mercaptobenzothiazolyl)-(methyl 6-O-tertbutyldiphenylsilyl-2-deoxy-α-D-glucopyranosid-2-yl)-isophthalate

There total 3 articles about (2-Mercaptobenzothiazolyl)-(methyl 6-O-tertbutyldiphenylsilyl-2-deoxy-α-D-glucopyranosid-2-yl)-isophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 58479-62-2
(2R,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-tetrahydro-pyran-3,4,5-triol

: 261967-72-0
3-(2-Mercapto-benzothiazolylcarbonyl)-benzoyl chloride

: 261967-58-2
(2-Mercaptobenzothiazolyl)-(methyl 6-O-tertbutyldiphenylsilyl-2-deoxy-α-D-glucopyranosid-2-yl)-isophthalate

Guidance literature:: (2R,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-tetrahydro-pyran-3,4,5-triol; With di(n-butyl)tin oxide; In toluene; Heating; microwave irradiation;

3-(2-Mercapto-benzothiazolylcarbonyl)-benzoyl chloride; In toluene; for 4h;

Reference yield:

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 261967-58-2
(2-Mercaptobenzothiazolyl)-(methyl 6-O-tertbutyldiphenylsilyl-2-deoxy-α-D-glucopyranosid-2-yl)-isophthalate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₃N / toluene / 4 h / 20 °C

2.1: nBu₂SnO / toluene / Heating; microwave irradiation

2.2: 75 percent / toluene / 4 h

With di(n-butyl)tin oxide; triethylamine; In toluene; 1.1: Esterification / 2.1: Metallation / 2.2: Esterification;

Reference yield:

: 99-63-8
benzene-1,3-dicarbonyl dichloride

: 261967-58-2
(2-Mercaptobenzothiazolyl)-(methyl 6-O-tertbutyldiphenylsilyl-2-deoxy-α-D-glucopyranosid-2-yl)-isophthalate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₃N / toluene / 4 h / 20 °C

2.1: nBu₂SnO / toluene / Heating; microwave irradiation

2.2: 75 percent / toluene / 4 h

With di(n-butyl)tin oxide; triethylamine; In toluene; 1.1: Esterification / 2.1: Metallation / 2.2: Esterification;