2,9-dicyclohexyl-10-nitrophenanthrene

Base Information

Chemical Name:2,9-dicyclohexyl-10-nitrophenanthrene
CAS No.:605686-23-5
Molecular Formula:C₂₆H₂₉NO₂
Molecular Weight:387.522
Hs Code.:

Synonyms:2,9-dicyclohexyl-10-nitrophenanthrene

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Chemical Property of 2,9-dicyclohexyl-10-nitrophenanthrene

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Technology Process of 2,9-dicyclohexyl-10-nitrophenanthrene

There total 1 articles about 2,9-dicyclohexyl-10-nitrophenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 17024-21-4
9-Bromo-10-nitrophenanthrene

: 87100-15-0
cyclohexylboronic acid pinacol ester

: 605686-23-5
2,9-dicyclohexyl-10-nitrophenanthrene

Guidance literature:: 9-Bromo-10-nitrophenanthrene; With N-Bromosuccinimide; In tetrahydrofuran; acetone; at -30 ℃; for 5h; UV-irradiation;

cyclohexylboronic acid pinacol ester; With sodium hydrogencarbonate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride; palladium diacetate; In tetrahydrofuran; water; at 50 ℃; for 3h;
DOI:10.1021/ol035147k

Reference yield: 98.0%

: 605686-23-5
2,9-dicyclohexyl-10-nitrophenanthrene

: 605686-24-6
2,9-dicyclohexyl-10-aminophenanthrene

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 8h;
DOI:10.1021/ol035147k

Reference yield:

: 605686-23-5
2,9-dicyclohexyl-10-nitrophenanthrene

: N,N'-bis(2,9-dicyclohexyl-10-phenanthrenyl)-4,5-dihydroimidazolium chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / H₂ / Pd/C / methanol / 8 h

2: 75 percent / propan-1-ol; H₂O / 20 h / 20 - 60 °C

3: 81 percent / NaBH₄ / tetrahydrofuran

4: 85 percent / formic acid / 60 h / Heating

With sodium tetrahydroborate; formic acid; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; propan-1-ol; water;
DOI:10.1021/ol035147k