potassium syn-(R)-1-phenylethanediazoate

Base Information

Chemical Name:potassium syn-(R)-1-phenylethanediazoate
CAS No.:29882-69-7
Molecular Formula:C₈H₉N₂O*K
Molecular Weight:188.271
Hs Code.:

Synonyms:potassium syn-(R)-1-phenylethanediazoate

Suppliers and Price of potassium syn-(R)-1-phenylethanediazoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of potassium syn-(R)-1-phenylethanediazoate

Chemical Property:

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

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Technology Process of potassium syn-(R)-1-phenylethanediazoate

There total 5 articles about potassium syn-(R)-1-phenylethanediazoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 143678-71-1
(+)-(R)-ethyl N-nitroso-N-(1-phenylethyl)carbamate

: 29882-69-7
potassium syn-(R)-1-phenylethanediazoate

Guidance literature:: With potassium tert-butylate; In diethyl ether; at 0 ℃; for 0.333333h;

Reference yield: 59.0%

: 143591-22-4
(-)-(R)-N-(1-phenylethyl)-N-nitrosohydrazine

: 29882-69-7
potassium anti-(R)-1-phenylethanediazoate

Guidance literature:: With potassium methanolate; isopentyl nitrite; In methanol; diethyl ether; at 0 ℃; for 1.5h;

Reference yield:

: 14185-43-4
(R)-(1-phenylethyl)-carbamic acid ethyl ester

: 29882-69-7
potassium syn-(R)-1-phenylethanediazoate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / N₂O₄, sodium acetate / CH₂Cl₂ / -50 °C

2: 83 percent / t-BuOK / diethyl ether / 0.33 h / 0 °C

With potassium tert-butylate; sodium acetate; dinitrogen tetraoxide; In diethyl ether; dichloromethane;