3,3-Dimethyl-7,9,12-triphenyl-4,10,11-trioxa-12-aza-tricyclo[7.2.1.0^1,6]dodecane

Base Information

• Chemical Name: 3,3-Dimethyl-7,9,12-triphenyl-4,10,11-trioxa-12-aza-tricyclo[7.2.1.0^1,6]dodecane
• CAS No.: 97933-98-7
• Molecular Formula: C₂₈H₂₉NO₃
• Molecular Weight: 427.543

Synonyms:3,3-Dimethyl-7,9,12-triphenyl-4,10,11-trioxa-12-aza-tricyclo[7.2.1.0^1,6]dodecane

Chemical Property of 3,3-Dimethyl-7,9,12-triphenyl-4,10,11-trioxa-12-aza-tricyclo[7.2.1.0^1,6]dodecane

Chemical Property:

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Technology Process of 3,3-Dimethyl-7,9,12-triphenyl-4,10,11-trioxa-12-aza-tricyclo[7.2.1.0^1,6]dodecane

There total 3 articles about 3,3-Dimethyl-7,9,12-triphenyl-4,10,11-trioxa-12-aza-tricyclo[7.2.1.0^1,6]dodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

1,2,4-Triphenyl-7,7-dimethyl-6-oxa-1,4,5,6,7,8-hexahydroquinoline (97933-90-9) → 3,3-Dimethyl-7,9,12-triphenyl-4,10,11-trioxa-12-aza-tricyclo[7.2.1.01,6]dodecane (97933-98-7)

Guidance literature:

With dihydrogen peroxide; sodium acetate; In acetic acid; at 35 - 40 ℃;

DOI:10.1007/BF00505905

Reference yield:

2,2-dimethyl-5-(3-oxo-1,3-diphenyl-propyl)-tetrahydro-pyran-4-one (39744-96-2) → 3,3-Dimethyl-7,9,12-triphenyl-4,10,11-trioxa-12-aza-tricyclo[7.2.1.01,6]dodecane (97933-98-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / p-toluenesulfonic acid / xylene / 4 h / Heating

2: 52 percent / H₂O₂, sodium acetate / acetic acid / 35 - 40 °C

With dihydrogen peroxide; sodium acetate; toluene-4-sulfonic acid; In acetic acid; xylene;

DOI:10.1007/BF00505905

Reference yield:

aniline (62-53-3) → 3,3-Dimethyl-7,9,12-triphenyl-4,10,11-trioxa-12-aza-tricyclo[7.2.1.01,6]dodecane (97933-98-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / p-toluenesulfonic acid / xylene / 4 h / Heating

2: 52 percent / H₂O₂, sodium acetate / acetic acid / 35 - 40 °C

With dihydrogen peroxide; sodium acetate; toluene-4-sulfonic acid; In acetic acid; xylene;

DOI:10.1007/BF00505905

upstream raw materials:

1,2,4-Triphenyl-7,7-dimethyl-6-oxa-1,4,5,6,7,8-hexahydroquinoline

2,2-dimethyl-5-(3-oxo-1,3-diphenyl-propyl)-tetrahydro-pyran-4-one

aniline

Downstream raw materials:

2,2-Dimethyl-6-(3-oxo-1,3-diphenyl-propyl)-4-phenyl-[1,4]oxazepan-5-one

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