5,7-diphenyldibenzazepin-5-ol

Base Information

Chemical Name:5,7-diphenyldibenzazepin-5-ol
CAS No.:106569-20-4
Molecular Formula:C₂₆H₁₉NO
Molecular Weight:361.443
Hs Code.:

Synonyms:5,7-diphenyldibenzazepin-5-ol

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Chemical Property of 5,7-diphenyldibenzazepin-5-ol

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Technology Process of 5,7-diphenyldibenzazepin-5-ol

There total 3 articles about 5,7-diphenyldibenzazepin-5-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 106569-03-3
5,7-diphenyl-5H-dibenzazepine

: 106569-20-4
5,7-diphenyldibenzazepin-5-ol

Guidance literature:: With sodium hydroxide; air; tetrabutylammomium bromide; In chlorobenzene; at 60 - 85 ℃; for 24h;
DOI:10.1021/jo00380a010

Reference yield:

: [2'-(Amino-phenyl-methyl)-biphenyl-2-yl]-phenyl-methanone

: 106569-20-4
5,7-diphenyldibenzazepin-5-ol

Guidance literature:: Multi-step reaction with 2 steps

1: aq. 4-toluenesulfonic acid / acetone / 10 h / Heating

2: 83 percent / 50percent aq. NaOH, tetrabutylammonium bromide, air / chlorobenzene / 24 h / 60 - 85 °C

With sodium hydroxide; air; tetrabutylammomium bromide; toluene-4-sulfonic acid; In chlorobenzene; acetone;
DOI:10.1021/jo00380a010

Reference yield:

: 106568-98-3,106568-99-4
<2'-(2-phenyl-1,3-dioxolan-2-yl)<1,1'-biphenyl>-2-yl>phenylmethanone oxime

: 106569-20-4
5,7-diphenyldibenzazepin-5-ol

Guidance literature:: Multi-step reaction with 3 steps

1: Zn, concd. NH₃, ammonium aceatate / Heating

2: aq. 4-toluenesulfonic acid / acetone / 10 h / Heating

3: 83 percent / 50percent aq. NaOH, tetrabutylammonium bromide, air / chlorobenzene / 24 h / 60 - 85 °C

With ammonium hydroxide; sodium hydroxide; air; ammonium acetate; tetrabutylammomium bromide; toluene-4-sulfonic acid; zinc; In chlorobenzene; acetone;
DOI:10.1021/jo00380a010