(Z)-2-benzoyloxy-6-O-(2,3,5,6-tetraO-benzoyl-β-D-galactofuranosyl)-2,4-hexadien-4-olide

Base Information

• Chemical Name: (Z)-2-benzoyloxy-6-O-(2,3,5,6-tetraO-benzoyl-β-D-galactofuranosyl)-2,4-hexadien-4-olide
• CAS No.: 138760-78-8
• Molecular Formula: C₄₇H₃₆O₁₄
• Molecular Weight: 824.794
• Mol file: 138760-78-8.mol

Synonyms:(Z)-2-benzoyloxy-6-O-(2,3,5,6-tetraO-benzoyl-β-D-galactofuranosyl)-2,4-hexadien-4-olide

Chemical Property of (Z)-2-benzoyloxy-6-O-(2,3,5,6-tetraO-benzoyl-β-D-galactofuranosyl)-2,4-hexadien-4-olide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-2-benzoyloxy-6-O-(2,3,5,6-tetraO-benzoyl-β-D-galactofuranosyl)-2,4-hexadien-4-olide

There total 1 articles about (Z)-2-benzoyloxy-6-O-(2,3,5,6-tetraO-benzoyl-β-D-galactofuranosyl)-2,4-hexadien-4-olide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

2,3,5-tri-O-benzoyl-6-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-D-galactono-1,4-lactone (124662-83-5) → (E)-2-benzoyloxy-6-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2,4-hexadien-4-olide (138760-77-7) + (Z)-2-benzoyloxy-6-O-(2,3,5,6-tetraO-benzoyl-β-D-galactofuranosyl)-2,4-hexadien-4-olide (138760-78-8)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 0 ℃; for 2h;

DOI:10.1016/0008-6215(91)80012-C

Reference yield:

2-O-benzoyloxy-6-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2,4-hexadien-4-olide (138760-77-7,138760-78-8) → 2(R),4(S)-2-O-benzoyl-3,5-dideoxy-6-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-hexono-1,4-lactone (138760-81-3) + 2(S),4(R)-2-O-benzoyl-3,5-dideoxy-6-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-hexono-1,4-lactone (138760-80-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; at 0 ℃; for 3h;

DOI:10.1016/0008-6215(91)80012-C

upstream raw materials:

2,3,5-tri-O-benzoyl-6-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-D-galactono-1,4-lactone

Downstream raw materials:

2(R),4(S)-2-O-benzoyl-3,5-dideoxy-6-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-hexono-1,4-lactone

2(S),4(R)-2-O-benzoyl-3,5-dideoxy-6-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-hexono-1,4-lactone