(2S,2'S)-tetra-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))dipentanedioate

Base Information

Chemical Name:(2S,2'S)-tetra-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))dipentanedioate
CAS No.:1446011-81-9
Molecular Formula:C₄₀H₆₂N₈O₁₀S
Molecular Weight:847.046
Hs Code.:

Synonyms:(2S,2'S)-tetra-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))dipentanedioate

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Chemical Property of (2S,2'S)-tetra-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))dipentanedioate

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Technology Process of (2S,2'S)-tetra-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))dipentanedioate

There total 2 articles about (2S,2'S)-tetra-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))dipentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1262483-37-3
(S)-di-tert-butyl 2-azidopentanedioate

: 1446011-78-4
4-(2-(di(prop-2-yn-1-yl)amino)ethyl)benzenesulfonamide

: 1446011-81-9
(2S,2'S)-tetra-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))dipentanedioate

Guidance literature:: With copper; copper(II) sulfate; In tetrahydrofuran; water; at 20 ℃; for 3h;

Reference yield:

: 35303-76-5
4-(2-aminoethyl)benzenesulfonamide

: 1446011-81-9
(2S,2'S)-tetra-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))dipentanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile; toluene / 20 °C

2: copper; copper(II) sulfate / tetrahydrofuran; water / 3 h / 20 °C

With copper; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; toluene; acetonitrile;

Reference yield: 45.0%

: (NEt₄)2[rhenium(I)(bromide)3(carbonyl)3]

: 1446011-81-9
(2S,2'S)-tetra-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))dipentanedioate

: C₂₇H₃₀N₈O₁₃ReS⁽¹⁺⁾

Guidance literature:: (NEt₄)2[rhenium(I)(bromide)3(carbonyl)3]; (2S,2'S)-tetra-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))dipentanedioate; In acetonitrile; at 85 ℃; Inert atmosphere; Autoclave;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;