benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-D-glycero-α-D-manno-heptopyranoside

Base Information

Chemical Name:benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-D-glycero-α-D-manno-heptopyranoside
CAS No.:1554004-82-8
Molecular Formula:C₅₆H₅₇O₁₀P
Molecular Weight:921.036
Hs Code.:

Synonyms:benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-D-glycero-α-D-manno-heptopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-D-glycero-α-D-manno-heptopyranoside

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Technology Process of benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-D-glycero-α-D-manno-heptopyranoside

There total 3 articles about benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-D-glycero-α-D-manno-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₆H₅₇O₉P

: 1554004-82-8
benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-D-glycero-α-D-manno-heptopyranoside

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; at -20 - 20 ℃;
DOI:10.1016/j.bmc.2013.12.019

Reference yield:

: 1554004-78-2
benzyl 2,3,4,6-O-tetra-benzyl-D-glycero-α-D-mannoheptopyranoside

: 1554004-82-8
benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-D-glycero-α-D-manno-heptopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-tetrazole / dichloromethane; acetonitrile / 0.5 h / 20 °C / Molecular sieve

1.2: 2 h / 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; acetonitrile / -20 - 20 °C

With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2013.12.019

Reference yield:

: benzyl 7-O-tetra-butyldiphenylsilyl-2,3,4,6-O-tetra-benzyl-D-glycero-α-D-mannoheptopyranoside

: 1554004-82-8
benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-D-glycero-α-D-manno-heptopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

2.1: 1H-tetrazole / dichloromethane; acetonitrile / 0.5 h / 20 °C / Molecular sieve

2.2: 2 h / 20 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; acetonitrile / -20 - 20 °C

With 1H-tetrazole; tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2013.12.019