cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine-P-borane

Base Information

Chemical Name:cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine-P-borane
CAS No.:1428980-28-2
Molecular Formula:C₁₇H₃₂BPSi
Molecular Weight:306.311
Hs Code.:

Synonyms:cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine-P-borane

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Chemical Property of cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine-P-borane

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Technology Process of cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine-P-borane

There total 1 articles about cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine-P-borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1833-31-4
benzyl(chloro)dimethylsilane

: 203000-47-9
cyclohexyl(dimethyl)phosphine-borane

: 1428980-28-2
cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine-P-borane

Guidance literature:: cyclohexyl(dimethyl)phosphine-borane; With sec.-butyllithium; (-)-sparteine; In diethyl ether; at -78 ℃; for 3h; Inert atmosphere; Schlenk technique;

benzyl(chloro)dimethylsilane; In diethyl ether; at -78 ℃; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/om3012294

Reference yield:

: 1428980-28-2
cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine-P-borane

: cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine

Guidance literature:: cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine-P-borane; With tetrafluoroboric acid diethyl ether; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

With sodium hydrogencarbonate; In dichloromethane; water; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1021/om3012294

Reference yield:

: 1428980-28-2
cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine-P-borane

: BF₄^(1-)*C₁₇H₂₉PSi*H⁽¹⁺⁾

Guidance literature:: With tetrafluoroboric acid diethyl ether; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1021/om3012294