butyl-phenethyl sulfone

Base Information

• Chemical Name: butyl-phenethyl sulfone
• CAS No.: 100520-55-6
• Molecular Formula: C₁₂H₁₈O₂S
• Molecular Weight: 226.34
• Mol file: 100520-55-6.mol

Synonyms:butyl-phenethyl sulfone

Chemical Property of butyl-phenethyl sulfone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of butyl-phenethyl sulfone

There total 5 articles about butyl-phenethyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C19H22O3S → butyl-phenethyl sulfone (100520-55-6)

Guidance literature:

C₁₉H₂₂O₃S; With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at 20 ℃; for 0.166667h;

With sodium hydride; In tetrahydrofuran; hexane; mineral oil; at 20 ℃; for 8h;

DOI:10.1055/s-0033-1339117

Reference yield: 57.0%

1-iodo-butane (542-69-8) + 2-phenylethyl tosylate (4455-09-8) → butyl-phenethyl sulfone (100520-55-6)

Guidance literature:

With sodium metabisulfite; tetrabutylammomium bromide; potassium formate; caesium carbonate; In dimethyl sulfoxide; at 100 ℃; for 10h; Inert atmosphere;

Reference yield:

1-(1-butylthio)-2-phenylethane (14679-16-4) → butyl-phenethyl sulfone (100520-55-6)

Guidance literature:

With dihydrogen peroxide; acetic acid;

upstream raw materials:

1-(1-butylthio)-2-phenylethane

styrene

1-phenyl-2-bromoethane

1-iodo-butane