Technology Process of C40H34O4S
There total 6 articles about C40H34O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 60 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: aluminum (III) chloride / dichloromethane / 2 h / 0 °C
2: N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bis-(diphenylphosphino)ferrocene / toluene / 3 h / Inert atmosphere; Reflux
3: potassium tert-butylate / tetrahydrofuran / 1 h
4: sodium acetate / toluene / 3 h / Reflux
5: sodium hydroxide; water / methanol / 3 h / Reflux
6: potassium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C
With
aluminum (III) chloride; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate; water; sodium acetate; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium tert-butylate / tetrahydrofuran / 1 h
2: sodium acetate / toluene / 3 h / Reflux
3: sodium hydroxide; water / methanol / 3 h / Reflux
4: potassium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C
With
potassium tert-butylate; water; sodium acetate; potassium carbonate; sodium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;
