C₃₃H₄₆O₅Si

Base Information

Chemical Name:C₃₃H₄₆O₅Si
CAS No.:615249-28-0
Molecular Formula:C₃₃H₄₆O₅Si
Molecular Weight:550.811
Hs Code.:

C<sub>33</sub>H<sub>46</sub>O<sub>5</sub>Si

Synonyms:C₃₃H₄₆O₅Si

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Chemical Property of C₃₃H₄₆O₅Si

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Technology Process of C₃₃H₄₆O₅Si

There total 25 articles about C₃₃H₄₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 615249-39-3
C₂₈H₄₁F₃O₈SSi

: 98-80-6
phenylboronic acid

: 615249-28-0
C₃₃H₄₆O₅Si

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In methanol; N,N-dimethyl-formamide; at 80 ℃; for 1h;
DOI:10.1002/anie.200351744

Reference yield:

: 154278-40-7
(1S,2S,4S)-bicyclo[2.2.1]hept-5-en-2-yl acetate

: 615249-28-0
C₃₃H₄₆O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / p-TsOH / methanol / 3 h / 25 °C

2: 57 percent / TMSOTf; iPr₂NEt / CH₂Cl₂ / 16 h / -20 - 25 °C

3: 57 percent / Br₂; N,N-dimethylaniline / CH₂Cl₂ / 12 h / -78 - 0 °C

4: 75 percent / nBu₃SnH; AIBN / toluene / 15 h / 110 °C

5: 65 percent / KHMDS / tetrahydrofuran / 1 h / -78 °C

6: 78 percent / Pd(PPh₃)4; Cs₂CO₃ / dimethylformamide; methanol / 1 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2'-azobis(isobutyronitrile); trimethylsilyl trifluoromethanesulfonate; bromine; tri-n-butyl-tin hydride; potassium hexamethylsilazane; caesium carbonate; toluene-4-sulfonic acid; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; 7: Suzuki reaction;
DOI:10.1002/anie.200351744

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 615249-28-0
C₃₃H₄₆O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1: 72 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 25 °C

2: 97 percent / Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 3 h / 25 °C

3: 78 percent / tetrahydrofuran / 12 h / 25 °C

4: 50 percent / SeO₂; t-BuOOH / CH₂Cl₂ / 6 h / 25 °C

5: 57 percent / Br₂; N,N-dimethylaniline / CH₂Cl₂ / 12 h / -78 - 0 °C

6: 75 percent / nBu₃SnH; AIBN / toluene / 15 h / 110 °C

7: 65 percent / KHMDS / tetrahydrofuran / 1 h / -78 °C

8: 78 percent / Pd(PPh₃)4; Cs₂CO₃ / dimethylformamide; methanol / 1 h / 80 °C

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; selenium(IV) oxide; 2,2'-azobis(isobutyronitrile); bromine; tri-n-butyl-tin hydride; potassium hexamethylsilazane; sodium hydrogencarbonate; caesium carbonate; Dess-Martin periodane; N,N-dimethyl-aniline; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; 2: Dess-martin oxidation / 3: Wittig reaction / 8: Suzuki reaction;
DOI:10.1002/anie.200351744