(E)-N-cyclohexyl-2-[N-benzyl-N-(2-nitrobenzoyl)amino]-3-hydroxy-3-phenylacrylamide

Base Information

• Chemical Name: (E)-N-cyclohexyl-2-[N-benzyl-N-(2-nitrobenzoyl)amino]-3-hydroxy-3-phenylacrylamide
• CAS No.: 1616366-96-1
• Molecular Formula: C₂₉H₂₉N₃O₅
• Molecular Weight: 499.566

Synonyms:(E)-N-cyclohexyl-2-[N-benzyl-N-(2-nitrobenzoyl)amino]-3-hydroxy-3-phenylacrylamide

Chemical Property of (E)-N-cyclohexyl-2-[N-benzyl-N-(2-nitrobenzoyl)amino]-3-hydroxy-3-phenylacrylamide

Chemical Property:

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Technology Process of (E)-N-cyclohexyl-2-[N-benzyl-N-(2-nitrobenzoyl)amino]-3-hydroxy-3-phenylacrylamide

There total 1 articles about (E)-N-cyclohexyl-2-[N-benzyl-N-(2-nitrobenzoyl)amino]-3-hydroxy-3-phenylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

Cyclohexyl isocyanide (931-53-3) + phenylglyoxal hydrate (1074-12-0) + ortho-nitrobenzoic acid (552-16-9,104810-18-6) + benzylamine (100-46-9) → (E)-N-cyclohexyl-2-[N-benzyl-N-(2-nitrobenzoyl)amino]-3-hydroxy-3-phenylacrylamide (1616366-96-1)

Guidance literature:

phenylglyoxal hydrate; benzylamine; In methanol; at 20 ℃; for 0.25h;

Cyclohexyl isocyanide; ortho-nitrobenzoic acid; In methanol; at 20 ℃; for 24h;

DOI:10.1039/c4ob00444b

Reference yield: 85.0%

(E)-N-cyclohexyl-2-[N-benzyl-N-(2-nitrobenzoyl)amino]-3-hydroxy-3-phenylacrylamide (1616366-96-1) → N-cyclohexyl-4-benzyl-5-oxo-2-phenyl-3,4-dihydrobenzo[e][1,4]diazepine-3-carboxamide (1123339-22-9)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; In ethanol; for 0.75h; Reflux;

DOI:10.1039/c4ob00444b

upstream raw materials:

Cyclohexyl isocyanide

phenylglyoxal hydrate

ortho-nitrobenzoic acid

benzylamine

Downstream raw materials:

N-cyclohexyl-4-benzyl-5-oxo-2-phenyl-3,4-dihydrobenzo[e][1,4]diazepine-3-carboxamide

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