N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-6-methoxy-1,3,5-triazine-2,4-diamine

Base Information

Chemical Name:N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-6-methoxy-1,3,5-triazine-2,4-diamine
CAS No.:1352803-97-4
Molecular Formula:C₂₅H₃₂N₆O
Molecular Weight:432.569
Hs Code.:

N<sub>2</sub>-(1-benzylpiperidin-4-yl)-N<sub>4</sub>-mesityl-6-methoxy-1,3,5-triazine-2,4-diamine

Synonyms:N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-6-methoxy-1,3,5-triazine-2,4-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-6-methoxy-1,3,5-triazine-2,4-diamine

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Technology Process of N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-6-methoxy-1,3,5-triazine-2,4-diamine

There total 5 articles about N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-6-methoxy-1,3,5-triazine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.7%

: 1352804-12-6
N₂-mesityl-6-methoxy-N₄-(piperidin-4-yl)-1,3,5-triazine-2,4-diamine

: 1352803-97-4
N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-6-methoxy-1,3,5-triazine-2,4-diamine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.ejmech.2012.02.019

Reference yield:

: 1352804-07-9
6-chloro-N₂-mesityl-N₄-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine

: 1352803-97-4
N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-6-methoxy-1,3,5-triazine-2,4-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium / 4 h / 60 °C

2.1: trifluoroacetic acid / dichloromethane / 20 °C

2.2: pH 8

3.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

With sodium; potassium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.02.019

Reference yield:

: 88-05-1
2,4,6-trimethylaniline

: 1352803-97-4
N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-6-methoxy-1,3,5-triazine-2,4-diamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / tetrahydrofuran / 3 h / 0 °C

2.1: sodium hydrogencarbonate / tetrahydrofuran; water; acetone / 8 h / 30 °C

3.1: sodium / 4 h / 60 °C

4.1: trifluoroacetic acid / dichloromethane / 20 °C

4.2: pH 8

5.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

With sodium; sodium hydrogencarbonate; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.ejmech.2012.02.019