4-[4-(perflurohexylsulfonyl)phenylazo]-N-[8-(methacryloyloxy)octyl]-N-octylaniline

Base Information

Chemical Name:4-[4-(perflurohexylsulfonyl)phenylazo]-N-[8-(methacryloyloxy)octyl]-N-octylaniline
CAS No.:202392-86-7
Molecular Formula:C₃₈H₄₆F₁₃N₃O₄S
Molecular Weight:887.846
Hs Code.:

Synonyms:4-[4-(perflurohexylsulfonyl)phenylazo]-N-[8-(methacryloyloxy)octyl]-N-octylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[4-(perflurohexylsulfonyl)phenylazo]-N-[8-(methacryloyloxy)octyl]-N-octylaniline

Chemical Property:

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Technology Process of 4-[4-(perflurohexylsulfonyl)phenylazo]-N-[8-(methacryloyloxy)octyl]-N-octylaniline

There total 3 articles about 4-[4-(perflurohexylsulfonyl)phenylazo]-N-[8-(methacryloyloxy)octyl]-N-octylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 4-[4-(perflurohexylsulfonyl)phenylazo]-N-(8-hydroxyoctyl)-N-octylaniline

: 920-46-7,26937-45-1
Methacryloyl chloride

: 202392-86-7
4-[4-(perflurohexylsulfonyl)phenylazo]-N-[8-(methacryloyloxy)octyl]-N-octylaniline

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃;
DOI:10.1246/bcsj.70.3153

Reference yield:

: 147029-28-5
4-(Perfluorohexylsulfonyl)aniline

: 202392-86-7
4-[4-(perflurohexylsulfonyl)phenylazo]-N-[8-(methacryloyloxy)octyl]-N-octylaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: conc. hydrochloric acid; sodium nitrite / acetone; H₂O / 1 h / 0 °C

1.2: 46 percent / acetone; H₂O / 2 h / 0 °C

2.1: 55 percent / triethylamine / tetrahydrofuran / 0 °C

With hydrogenchloride; triethylamine; sodium nitrite; In tetrahydrofuran; water; acetone; 1.1: Diazotization / 1.2: coupling / 2.1: Acylation;
DOI:10.1246/bcsj.70.3153

Reference yield:

: 8-(octyl-phenyl-amino)-octan-1-ol

: 202392-86-7
4-[4-(perflurohexylsulfonyl)phenylazo]-N-[8-(methacryloyloxy)octyl]-N-octylaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: conc. hydrochloric acid; sodium nitrite / acetone; H₂O / 1 h / 0 °C

1.2: 46 percent / acetone; H₂O / 2 h / 0 °C

2.1: 55 percent / triethylamine / tetrahydrofuran / 0 °C

With hydrogenchloride; triethylamine; sodium nitrite; In tetrahydrofuran; water; acetone; 1.1: Diazotization / 1.2: coupling / 2.1: Acylation;
DOI:10.1246/bcsj.70.3153