6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methylpyrimidine-2,4,5(3H)-trione-5-hydrazone

Base Information

Chemical Name:6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methylpyrimidine-2,4,5(3H)-trione-5-hydrazone
CAS No.:79854-14-1
Molecular Formula:C₁₆H₂₂N₆O₂
Molecular Weight:330.39
Hs Code.:

Synonyms:6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methylpyrimidine-2,4,5(3H)-trione-5-hydrazone

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Chemical Property of 6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methylpyrimidine-2,4,5(3H)-trione-5-hydrazone

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Technology Process of 6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methylpyrimidine-2,4,5(3H)-trione-5-hydrazone

There total 9 articles about 6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methylpyrimidine-2,4,5(3H)-trione-5-hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54929-07-6
N-formyl-N,N',N',4,5-pentametyl-o-phenylenediamine

: 79854-14-1
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methylpyrimidine-2,4,5(3H)-trione-5-hydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid

2: 1.) N,N-dimethylaniline, 2.) acetic acid / 1.) methanol

3: 1.) hydrogen, 2.) sodium nitrite / 1.) palladium/10percent on charcoal / 1.) water, 2.) 1 h

4: triphenylphosphine

With sulfuric acid; hydrogen; acetic acid; N,N-dimethyl-aniline; triphenylphosphine; sodium nitrite; palladium on activated charcoal;
DOI:10.1021/ja00352a045

Reference yield:

: 85894-78-6
N,N',N',4,5-pentametyl-o-phenylenediamine

: 79854-14-1
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methylpyrimidine-2,4,5(3H)-trione-5-hydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N,N-dimethylaniline, 2.) acetic acid / 1.) methanol

2: 1.) hydrogen, 2.) sodium nitrite / 1.) palladium/10percent on charcoal / 1.) water, 2.) 1 h

3: triphenylphosphine

With hydrogen; acetic acid; N,N-dimethyl-aniline; triphenylphosphine; sodium nitrite; palladium on activated charcoal;
DOI:10.1021/ja00352a045

Reference yield:

: 79872-70-1
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methyl-5-nitrouracil

: 79854-14-1
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-3-methylpyrimidine-2,4,5(3H)-trione-5-hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hydrogen, 2.) sodium nitrite / 1.) palladium/10percent on charcoal / 1.) water, 2.) 1 h

2: triphenylphosphine

With hydrogen; triphenylphosphine; sodium nitrite; palladium on activated charcoal;
DOI:10.1021/ja00352a045