1D-(1,2,4/3,5)-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamido>-1-O-phosphono-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

Base Information

Chemical Name:1D-(1,2,4/3,5)-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamido>-1-O-phosphono-5-C-hydroxymethyl-1,3,4-cyclohexanetriol
CAS No.:143465-47-8
Molecular Formula:C₃₅H₆₈NO₁₁P
Molecular Weight:709.899
Hs Code.:

Synonyms:1D-(1,2,4/3,5)-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamido>-1-O-phosphono-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

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Chemical Property of 1D-(1,2,4/3,5)-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamido>-1-O-phosphono-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

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Technology Process of 1D-(1,2,4/3,5)-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamido>-1-O-phosphono-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

There total 31 articles about 1D-(1,2,4/3,5)-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamido>-1-O-phosphono-5-C-hydroxymethyl-1,3,4-cyclohexanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 143465-56-9
(R)-3-Hydroxy-tetradecanoic acid (1R,2R,3S,5R,6R)-3-(diphenoxy-phosphoryloxy)-6-hydroxy-5-hydroxymethyl-2-((R)-3-hydroxy-tetradecanoylamino)-cyclohexyl ester

: 143465-47-8
1D-(1,2,4/3,5)-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamido>-1-O-phosphono-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethanol; water;
DOI:10.1016/0040-4039(92)80009-9

Reference yield: 85.0%

: 152868-70-7
1D-(1,2,4/3,5)-4,7-O-benzylidene-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamido>-1-O-dibenzylphosphono-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

: 143465-47-8
1D-(1,2,4/3,5)-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamido>-1-O-phosphono-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; water; at 25 ℃; for 5h; under 750.06 Torr;
DOI:10.1016/S0040-4020(01)88023-6

Reference yield:

: (R)-3-Methoxymethoxy-tetradecanoic acid 2-oxo-2-phenyl-ethyl ester

: 143465-47-8
1D-(1,2,4/3,5)-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamido>-1-O-phosphono-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

Guidance literature:: Multi-step reaction with 7 steps

1: Zn dust / acetic acid

2: 92 percent / DCC / CH₂Cl₂

3: H₂ / 20percent Pd(OH)2 / tetrahydrofuran; methanol

4: 69 percent / CSA / dimethylformamide / Ambient temperature

5: 64 percent / DCC, DMAP / CH₂Cl₂ / Ambient temperature

6: 97 percent / HCl / methanol / 50 °C

7: 100 percent / H₂ / PtO₂ / H₂O; ethanol

With hydrogenchloride; dmap; camphor-10-sulfonic acid; hydrogen; dicyclohexyl-carbodiimide; zinc; platinum(IV) oxide; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(92)80009-9