2,8-bis(2,3-dimethoxybenzene-1-ylethynyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzodiazocine

Base Information

Chemical Name:2,8-bis(2,3-dimethoxybenzene-1-ylethynyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzodiazocine
CAS No.:1004754-45-3
Molecular Formula:C₃₇H₃₄N₂O₄
Molecular Weight:570.688
Hs Code.:

Synonyms:2,8-bis(2,3-dimethoxybenzene-1-ylethynyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzodiazocine

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Chemical Property of 2,8-bis(2,3-dimethoxybenzene-1-ylethynyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzodiazocine

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Technology Process of 2,8-bis(2,3-dimethoxybenzene-1-ylethynyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzodiazocine

There total 1 articles about 2,8-bis(2,3-dimethoxybenzene-1-ylethynyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzodiazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 171087-99-3
1-ethynyl-2,3-dimethoxybenzene

: 390357-37-6
(rac)-2,8-diiodo-4,10-dimethyl-5,11-methano-6H,12H-dibenzo[b,f][1,5]diazocine

: 1004754-45-3
2,8-bis(2,3-dimethoxybenzene-1-ylethynyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzodiazocine

Guidance literature:: With copper(l) iodide; diisopropylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; at 60 ℃; for 18h;
DOI:10.1002/ejoc.200700613