(2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(1-(4-((E)-(4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10,13-tetraoxo-8,14-dioxa-2,6,11-triazaheptadec-16-en-9-yl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate

Base Information

Chemical Name:(2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(1-(4-((E)-(4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10,13-tetraoxo-8,14-dioxa-2,6,11-triazaheptadec-16-en-9-yl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate
CAS No.:1448330-52-6
Molecular Formula:C₄₆H₅₅N₇O₁₅
Molecular Weight:945.981
Hs Code.:

(2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(1-(4-((E)-(4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10,13-tetraoxo-8,14-dioxa-2,6,11-triazaheptadec-16-en-9-yl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate

Synonyms:(2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(1-(4-((E)-(4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10,13-tetraoxo-8,14-dioxa-2,6,11-triazaheptadec-16-en-9-yl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate

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Chemical Property of (2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(1-(4-((E)-(4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10,13-tetraoxo-8,14-dioxa-2,6,11-triazaheptadec-16-en-9-yl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate

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Technology Process of (2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(1-(4-((E)-(4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10,13-tetraoxo-8,14-dioxa-2,6,11-triazaheptadec-16-en-9-yl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate

There total 8 articles about (2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(1-(4-((E)-(4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10,13-tetraoxo-8,14-dioxa-2,6,11-triazaheptadec-16-en-9-yl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1448330-51-5
(2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(2-((2-(allyloxy)-2-oxoethyl)amino)-1-(((4-nitrophenoxy)carbonyl)oxy)-2-oxoethyl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate

: 1316832-21-9
C₁₈H₂₃N₅O

: 1448330-52-6
(2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(1-(4-((E)-(4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10,13-tetraoxo-8,14-dioxa-2,6,11-triazaheptadec-16-en-9-yl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1039/c3cc42836b

Reference yield:

: 83025-11-0
3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl trichloroacetimidate

: 1448330-52-6
(2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(1-(4-((E)-(4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10,13-tetraoxo-8,14-dioxa-2,6,11-triazaheptadec-16-en-9-yl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane / 0.5 h / -20 °C / Molecular sieve

1.2: 2 h / -20 °C / Molecular sieve

2.1: 12 h / 20 °C

3.1: pyridine / dichloromethane / 6 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

With pyridine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3cc42836b

Reference yield:

: 1448330-49-1
(2R,3R,4R,5R,6R)-2-(acetoxymethyl)-6-(4-(2-((2-(allyloxy)-2-oxoethyl)amino)-1-hydroxy-2-oxoethyl)phenoxy)-5-azidotetrahydro-2H-pyran-3,4-diyl diacetate

: 1448330-52-6
(2R,3R,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-(4-(1-(4-((E)-(4-(dimethylamino)phenyl)diazenyl)phenyl)-1,7,10,13-tetraoxo-8,14-dioxa-2,6,11-triazaheptadec-16-en-9-yl)phenoxy)tetrahydro-2H-pyran-3,4-diyl diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 12 h / 20 °C

2: pyridine / dichloromethane / 6 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C

With pyridine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3cc42836b