tert-butyl (1S,2R)-2-nitro-1-(4-(trifluoromethyl)phenyl)propylcarbamate

Base Information

Chemical Name:tert-butyl (1S,2R)-2-nitro-1-(4-(trifluoromethyl)phenyl)propylcarbamate
CAS No.:1001022-98-5
Molecular Formula:C₁₅H₁₉F₃N₂O₄
Molecular Weight:348.322
Hs Code.:

Synonyms:tert-butyl (1S,2R)-2-nitro-1-(4-(trifluoromethyl)phenyl)propylcarbamate

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Chemical Property of tert-butyl (1S,2R)-2-nitro-1-(4-(trifluoromethyl)phenyl)propylcarbamate

Chemical Property:

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Technology Process of tert-butyl (1S,2R)-2-nitro-1-(4-(trifluoromethyl)phenyl)propylcarbamate

There total 2 articles about tert-butyl (1S,2R)-2-nitro-1-(4-(trifluoromethyl)phenyl)propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79-24-3
Nitroethane

: (E)-tert-butyl 4-(trifluoromethyl)benzylidenecarbamate

: 1001022-98-5
tert-butyl (1S,2R)-2-nitro-1-(4-(trifluoromethyl)phenyl)propylcarbamate

: tert-butyl (1R,2S)-2-nitro-1-(4-(trifluoromethyl)phenyl)propylcarbamate

Guidance literature:: With (H,Quin-BAM)*TfOH; at -20 ℃; Title compound not separated from byproducts;
DOI:10.1021/ja031906i

Reference yield:

: 871090-34-5
tert-butyl 4-(trifluoromethyl)benzylidenecarbamate

: 79-24-3
Nitroethane

: C₁₅H₁₉F₃N₂O₄

: 1001022-98-5
tert-butyl (1S,2R)-2-nitro-1-(4-(trifluoromethyl)phenyl)propylcarbamate

: tert-butyl (1R,2S)-2-nitro-1-(4-(trifluoromethyl)phenyl)propylcarbamate

Guidance literature:: tert-butyl 4-(trifluoromethyl)benzylidenecarbamate; Nitroethane; With ytterbium(III) isopropoxide; C₁₉H₂₀F₂N₂O₄; potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -60 ℃; for 20h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; toluene; optical yield given as %ee; Inert atmosphere;
DOI:10.3390/molecules15031280