C₃₃H₃₇NO₅

Base Information

Chemical Name:C₃₃H₃₇NO₅
CAS No.:1415722-86-9
Molecular Formula:C₃₃H₃₇NO₅
Molecular Weight:527.66
Hs Code.:

C<sub>33</sub>H<sub>37</sub>NO<sub>5</sub>

Synonyms:C₃₃H₃₇NO₅

Suppliers and Price of C₃₃H₃₇NO₅

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Chemical Property of C₃₃H₃₇NO₅

Chemical Property:

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Technology Process of C₃₃H₃₇NO₅

There total 6 articles about C₃₃H₃₇NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1415722-83-6,1415723-39-5
C₂₈H₂₉NO₅

: 870-63-3
prenyl bromide

: 1415722-86-9
C₃₃H₃₇NO₅

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In dichloromethane; water; at -5 - 20 ℃; for 17h; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.10.092

Reference yield:

: 57772-57-3
5-hydroxy-2-iodo-benzoic acid

: 1415722-86-9
C₃₃H₃₇NO₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / acetone / 5 h / Reflux; Inert atmosphere

2.1: potassium carbonate; copper / Triethylene glycol dimethyl ether / 48 h / 140 °C / Inert atmosphere

2.2: 15 h / 20 - 140 °C / Inert atmosphere

3.1: tetrahydrofuran; diethyl ether / -78 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

4.2: 19 h / 0 - 20 °C / Inert atmosphere

5.1: acetic acid; chromium(VI) oxide / water; acetone / 15 h / 20 °C / Inert atmosphere

6.1: benzene / 1 h / 20 °C / Inert atmosphere

7.1: platinum on carbon; hydrogen / ethyl acetate / 2.5 h / 20 °C / 760.05 Torr / Inert atmosphere

8.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / water; dichloromethane / 17 h / -5 - 20 °C / Inert atmosphere

With chromium(VI) oxide; platinum on carbon; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; copper; sodium hydride; potassium carbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; diethyl ether; Triethylene glycol dimethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; mineral oil; benzene;
DOI:10.1016/j.tetlet.2012.10.092

Reference yield:

: 1415684-40-0
C₂₁H₁₇IO₃

: 1415722-86-9
C₃₃H₃₇NO₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate; copper / Triethylene glycol dimethyl ether / 48 h / 140 °C / Inert atmosphere

1.2: 15 h / 20 - 140 °C / Inert atmosphere

2.1: tetrahydrofuran; diethyl ether / -78 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

3.2: 19 h / 0 - 20 °C / Inert atmosphere

4.1: acetic acid; chromium(VI) oxide / water; acetone / 15 h / 20 °C / Inert atmosphere

5.1: benzene / 1 h / 20 °C / Inert atmosphere

6.1: platinum on carbon; hydrogen / ethyl acetate / 2.5 h / 20 °C / 760.05 Torr / Inert atmosphere

7.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / water; dichloromethane / 17 h / -5 - 20 °C / Inert atmosphere

With chromium(VI) oxide; platinum on carbon; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; copper; sodium hydride; potassium carbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; diethyl ether; Triethylene glycol dimethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; mineral oil; benzene;
DOI:10.1016/j.tetlet.2012.10.092