Acetic acid (1S,2S,3S)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester

Base Information

• Chemical Name: Acetic acid (1S,2S,3S)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester
• CAS No.: 79549-63-6
• Molecular Formula: C₂₄H₃₃NO₉
• Molecular Weight: 479.527

Synonyms:Acetic acid (1S,2S,3S)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester

Chemical Property of Acetic acid (1S,2S,3S)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Technology Process of Acetic acid (1S,2S,3S)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester

There total 9 articles about Acetic acid (1S,2S,3S)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + 3-O-β-D-galactopyranosyl-(1→2)-β-D-glucuronopyranosylquillaic acid 28-O-α-L-rhamnopyranosyl-(1→2)-[β-D-glucopyranosyl-(1→3)]-4-O-acetyl-β-D-fucopyranosyl ester + acetic anhydride (108-24-7) → D-Fucose (3615-37-0,478518-52-4) + Acetic acid (1S,2S,3S)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester (79549-63-6) + Acetic acid (1R,2R,3R)-2,3,4-triacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester (79526-50-4,79549-65-8,79549-66-9,79549-67-0,79549-68-1,79617-01-9,83680-90-4,83680-91-5) + D-galactose (79526-50-4,79549-65-8,79549-66-9,79549-67-0,79549-68-1,79617-01-9,83680-90-4,83680-91-5) + quillaic acid-3-O-β-D-glucuronopyranoside

Guidance literature:

3-O-β-D-galactopyranosyl-(1→2)-β-D-glucuronopyranosylquillaic acid 28-O-α-L-rhamnopyranosyl-(1→2)-[β-D-glucopyranosyl-(1→3)]-4-O-acetyl-β-D-fucopyranosyl ester; With hydrogenchloride; In 1,4-dioxane; water; for 1h; Reflux;

(S)-1-phenyl-ethylamine; With sodium cyanoborohydride; In ethanol; water; at 40 ℃; for 4h;

acetic anhydride; With pyridine; at 20 ℃; for 24h;

DOI:10.1016/j.phytochem.2016.07.011

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + 3-O-β-D-galactopyranosyl-(1→2)-β-D-glucuronopyranosylquillaic acid 28-O-α-L-rhamnopyranosyl-(1→2)-[β-D-glucopyranosyl-(1→3)]-4-O-acetyl-β-D-fucopyranosyl ester + acetic anhydride (108-24-7) → C24H31NO11 + Acetic acid (1R,2S,3R)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester (79526-49-1,79549-62-5,79549-63-6,79549-64-7,83680-89-1) + Acetic acid (1S,2S,3S)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester (79549-63-6) + Acetic acid (1R,2R,3R)-2,3,4-triacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester (79526-50-4,79549-65-8,79549-66-9,79549-67-0,79549-68-1,79617-01-9,83680-90-4,83680-91-5) + D-galactose (79526-50-4,79549-65-8,79549-66-9,79549-67-0,79549-68-1,79617-01-9,83680-90-4,83680-91-5) + quillaic acid-3-O-β-D-glucuronopyranoside

Guidance literature:

3-O-β-D-galactopyranosyl-(1→2)-β-D-glucuronopyranosylquillaic acid 28-O-α-L-rhamnopyranosyl-(1→2)-[β-D-glucopyranosyl-(1→3)]-4-O-acetyl-β-D-fucopyranosyl ester; With trifluoroacetic acid; In water; for 1h; Reflux;

(S)-1-phenyl-ethylamine; With sodium cyanoborohydride; In ethanol; water; at 40 ℃; for 4h;

acetic anhydride; With pyridine; at 20 ℃; for 24h;

DOI:10.1016/j.phytochem.2016.07.011

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + 3-O-β-D-galactopyranosyl-(1→2)-β-D-glucuronopyranosylquillaic acid 28-O-α-L-rhamnopyranosyl-(1→2)-[β-D-glucopyranosyl-(1→3)]-4-O-acetyl-β-D-fucopyranosyl ester + acetic anhydride (108-24-7) → C24H31NO11 + Acetic acid (1R,2S,3R)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester (79526-49-1,79549-62-5,79549-63-6,79549-64-7,83680-89-1) + Acetic acid (1S,2S,3S)-2,3-diacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester (79549-63-6) + Acetic acid (1R,2R,3R)-2,3,4-triacetoxy-1-{(S)-1-acetoxy-2-[acetyl-((S)-1-phenyl-ethyl)-amino]-ethyl}-butyl ester (79526-50-4,79549-65-8,79549-66-9,79549-67-0,79549-68-1,79617-01-9,83680-90-4,83680-91-5) + D-galactose (79526-50-4,79549-65-8,79549-66-9,79549-67-0,79549-68-1,79617-01-9,83680-90-4,83680-91-5) + quillaic acid-3-O-β-D-glucuronopyranoside

Guidance literature:

3-O-β-D-galactopyranosyl-(1→2)-β-D-glucuronopyranosylquillaic acid 28-O-α-L-rhamnopyranosyl-(1→2)-[β-D-glucopyranosyl-(1→3)]-4-O-acetyl-β-D-fucopyranosyl ester; With trifluoroacetic acid; In water; for 1h; Reflux;

(S)-1-phenyl-ethylamine; With sodium cyanoborohydride; In ethanol; water; at 40 ℃; for 4h;

acetic anhydride; With pyridine; at 20 ℃; for 24h;

DOI:10.1016/j.phytochem.2016.07.011

upstream raw materials:

D-Fucose

(-)-α-methylbenzylamine

acetic anhydride

(S)-1-phenyl-ethylamine

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