methyl 8b-hydroxy-6-methoxy-3a-(4-methoxyphenyl)-1-oxo-3-phenyl-2,3-3a,8b-tetrahydro-cyclopenta[b]benzofuran-2-carboxylate

Base Information

Chemical Name:methyl 8b-hydroxy-6-methoxy-3a-(4-methoxyphenyl)-1-oxo-3-phenyl-2,3-3a,8b-tetrahydro-cyclopenta[b]benzofuran-2-carboxylate
CAS No.:1227475-82-2
Molecular Formula:C₂₇H₂₄O₇
Molecular Weight:460.483
Hs Code.:

Synonyms:methyl 8b-hydroxy-6-methoxy-3a-(4-methoxyphenyl)-1-oxo-3-phenyl-2,3-3a,8b-tetrahydro-cyclopenta[b]benzofuran-2-carboxylate

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Chemical Property of methyl 8b-hydroxy-6-methoxy-3a-(4-methoxyphenyl)-1-oxo-3-phenyl-2,3-3a,8b-tetrahydro-cyclopenta[b]benzofuran-2-carboxylate

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Technology Process of methyl 8b-hydroxy-6-methoxy-3a-(4-methoxyphenyl)-1-oxo-3-phenyl-2,3-3a,8b-tetrahydro-cyclopenta[b]benzofuran-2-carboxylate

There total 3 articles about methyl 8b-hydroxy-6-methoxy-3a-(4-methoxyphenyl)-1-oxo-3-phenyl-2,3-3a,8b-tetrahydro-cyclopenta[b]benzofuran-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228174-43-3
methyl 5-hydroxy-2,5-methano-8-methoxy-2-(4-methoxyphenyl)-10-oxo-3-phenyl-2,3,4,5-tetrahydro-1-benzoxepin-4-carboxylate

: 1227475-82-2
methyl 8b-hydroxy-6-methoxy-3a-(4-methoxyphenyl)-1-oxo-3-phenyl-2,3-3a,8b-tetrahydro-cyclopenta[b]benzofuran-2-carboxylate

Guidance literature:: With sodium methylate; In methanol; at 0 - 60 ℃; Inert atmosphere;
DOI:10.1021/jm101318b

Reference yield:

: 13198-99-7
3-hydroxy-7-methoxy-2-(4-methoxyphenyl)-4H-chromen-4-one

: 1227475-82-2
methyl 8b-hydroxy-6-methoxy-3a-(4-methoxyphenyl)-1-oxo-3-phenyl-2,3-3a,8b-tetrahydro-cyclopenta[b]benzofuran-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; dichloromethane / 15 h / 0 °C / Inert atmosphere; UV-irradiation

2: sodium methylate / methanol / 0 - 60 °C / Inert atmosphere

With sodium methylate; In methanol; dichloromethane;
DOI:10.1021/jm101318b

Reference yield:

: 103-26-4,1754-62-7
Methyl cinnamate

: 1227475-82-2
methyl 8b-hydroxy-6-methoxy-3a-(4-methoxyphenyl)-1-oxo-3-phenyl-2,3-3a,8b-tetrahydro-cyclopenta[b]benzofuran-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; dichloromethane / 15 h / 0 °C / Inert atmosphere; UV-irradiation

2: sodium methylate / methanol / 0 - 60 °C / Inert atmosphere

With sodium methylate; In methanol; dichloromethane;
DOI:10.1021/jm101318b