4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benzindole

Base Information

Chemical Name:4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benzindole
CAS No.:134745-87-2
Molecular Formula:C₁₈H₁₇NO₄S
Molecular Weight:343.403
Hs Code.:

4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benz<cd>indole

Synonyms:4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benzindole

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Chemical Property of 4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benzindole

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Technology Process of 4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benzindole

There total 3 articles about 4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 134745-86-1
1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole

: 134745-87-2
4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benzindole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 5 ℃; for 3h;
DOI:10.1248/cpb.39.23

Reference yield:

: 124465-55-0,51867-05-1
1-benzoyl-1,2,2a,3-tetrahydro-benz[cd]indole

: 134745-87-2
4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benzindole

Guidance literature:: Multi-step reaction with 3 steps

1: conc. hydrochloric acid / 8 h / Heating

2: triethylamine / benzene / 5 h / Heating

3: 90 percent / m-chloroperbenzoic acid / CHCl₃ / 3 h / 5 °C

With hydrogenchloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In chloroform; benzene;
DOI:10.1248/cpb.39.23

Reference yield:

: 1,2,2a,3-Tetrahydro-benzo[cd]indole

: 134745-87-2
4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benzindole

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / benzene / 5 h / Heating

2: 90 percent / m-chloroperbenzoic acid / CHCl₃ / 3 h / 5 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In chloroform; benzene;
DOI:10.1248/cpb.39.23