methyl (E)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-(2-methoxyphenyl)acrylate

Base Information

Chemical Name:methyl (E)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-(2-methoxyphenyl)acrylate
CAS No.:1373930-79-0
Molecular Formula:C₁₉H₁₉NO₅
Molecular Weight:341.364
Hs Code.:

Synonyms:methyl (E)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-(2-methoxyphenyl)acrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (E)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-(2-methoxyphenyl)acrylate

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Technology Process of methyl (E)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-(2-methoxyphenyl)acrylate

There total 2 articles about methyl (E)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-(2-methoxyphenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1373930-69-8
C₁₉H₁₈O₅

: 1373930-79-0
methyl (E)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-(2-methoxyphenyl)acrylate

Guidance literature:: With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; water; at 20 ℃; for 1.5h;
DOI:10.1055/s-0031-1289707

Reference yield:

: 139413-77-7
(Z)-2-Bromomethyl-3-(2-methoxy-phenyl)-acrylic acid methyl ester

: 1373930-79-0
methyl (E)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-(2-methoxyphenyl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 3 h / 20 °C

2: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 1.5 h / 20 °C

With hydroxylamine hydrochloride; potassium carbonate; sodium hydroxide; In ethanol; water; acetonitrile;
DOI:10.1055/s-0031-1289707

Reference yield: 80.0%

: 1373930-79-0
methyl (E)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-(2-methoxyphenyl)acrylate

: methyl 3-(2-methoxyphenyl)-3H-chromeno[4,3-c]isoxazole-3a(4H)-carboxylate

Guidance literature:: methyl (E)-2-({2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-(2-methoxyphenyl)acrylate; With N-chloro-succinimide; In tetrachloromethane; at 0 - 10 ℃; for 3h;

With triethylamine; In tetrachloromethane; at 20 ℃; for 2h;
DOI:10.1055/s-0031-1289707