C₁₆H₁₅NO₂

Base Information

• Chemical Name: C₁₆H₁₅NO₂
• CAS No.: 1176778-23-6
• Molecular Formula: C₁₆H₁₅NO₂
• Molecular Weight: 253.301

Synonyms:C₁₆H₁₅NO₂

Chemical Property of C₁₆H₁₅NO₂

Chemical Property:

Purity/Quality:

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Technology Process of C₁₆H₁₅NO₂

There total 5 articles about C₁₆H₁₅NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C18H17NO3 (1176778-21-4) → C16H15NO2 (1176778-23-6)

Guidance literature:

With methanol; potassium carbonate; at 20 ℃; for 24h;

DOI:10.1021/ja904534t

Reference yield:

C23H19NO3 → C16H15NO2 (1176778-23-6)

Guidance literature:

Multi-step reaction with 5 steps

1: sodium carbonate; (R,R)-N,N-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminochromium(III) chloride / benzene / 20 °C

2: palladium on activated charcoal; hydrogen

3: dmap

4: ammonium cerium (IV) nitrate

5: potassium carbonate; methanol

With methanol; dmap; ammonium cerium (IV) nitrate; (R,R)-N,N-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminochromium(III) chloride; palladium on activated charcoal; hydrogen; sodium carbonate; potassium carbonate; In benzene;

DOI:10.1039/c4cc10327k

Reference yield:

C23H21NO3 → C16H15NO2 (1176778-23-6)

Guidance literature:

Multi-step reaction with 3 steps

1: dmap

2: ammonium cerium (IV) nitrate

3: potassium carbonate; methanol

With methanol; dmap; ammonium cerium (IV) nitrate; potassium carbonate;

DOI:10.1039/c4cc10327k

upstream raw materials:

C₁₈H₁₇NO₃

Downstream raw materials:

(3S,5S)-3,5-diphenyl-3-pyrrolidinol

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