Technology Process of rel-(8R,14R)-9,10-dimethoxy-2,3-methylenedioxy-13-oxonorochotensane-7,8-carbolactone
There total 1 articles about rel-(8R,14R)-9,10-dimethoxy-2,3-methylenedioxy-13-oxonorochotensane-7,8-carbolactone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 70 percent / m-chloroperbenzoic acid / CH2Cl2 / 1.25 h / -30 - -25 °C
2: 70 percent / methanol / 0.83 h / Ambient temperature; Irradiation
3: 70 percent / benzene / 1 h / 80 °C
4: 71 percent / silver nitrate / acetone; H2O / 20 h / Heating
With
silver nitrate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; water; acetone; benzene;