2-ethoxycarbonylmethoxy-N,N-bis(ethoxycarbonylmethyl)benzene-1,4-diamine

Base Information

Chemical Name:2-ethoxycarbonylmethoxy-N,N-bis(ethoxycarbonylmethyl)benzene-1,4-diamine
CAS No.:864169-27-7
Molecular Formula:C₁₈H₂₆N₂O₇
Molecular Weight:382.414
Hs Code.:

Synonyms:2-ethoxycarbonylmethoxy-N,N-bis(ethoxycarbonylmethyl)benzene-1,4-diamine

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Chemical Property of 2-ethoxycarbonylmethoxy-N,N-bis(ethoxycarbonylmethyl)benzene-1,4-diamine

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Technology Process of 2-ethoxycarbonylmethoxy-N,N-bis(ethoxycarbonylmethyl)benzene-1,4-diamine

There total 4 articles about 2-ethoxycarbonylmethoxy-N,N-bis(ethoxycarbonylmethyl)benzene-1,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 864169-25-5
[(2-ethoxycarbonylmethoxy-4-nitro-phenyl)-ethoxycarbonylmethyl-amino]-acetic acid ethyl ester

: 864169-27-7
2-ethoxycarbonylmethoxy-N,N-bis(ethoxycarbonylmethyl)benzene-1,4-diamine

Guidance literature:: With hydrogen; palladium on activated charcoal; In diethyl ether; atmospheric pressure;
DOI:10.1055/s-2005-869900

Reference yield:

: 864169-18-6
[(2-ethoxycarbonylmethoxy-phenyl)-ethoxycarbonylmethyl-amino]acetic acid ethyl ester

: 864169-27-7
2-ethoxycarbonylmethoxy-N,N-bis(ethoxycarbonylmethyl)benzene-1,4-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / AcOH; HNO₃ / 0 °C

2: 63 percent / H₂ / Pd/C / diethyl ether / atmospheric pressure

With hydrogen; nitric acid; acetic acid; palladium on activated charcoal; In diethyl ether;
DOI:10.1055/s-2005-869900

Reference yield:

: trisodium o-aminophenol-N,N,O-triacetate

: 864169-27-7
2-ethoxycarbonylmethoxy-N,N-bis(ethoxycarbonylmethyl)benzene-1,4-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: 15.8 g / H₂SO₄ / 72 h / Heating

2: 51 percent / AcOH; HNO₃ / 0 °C

3: 63 percent / H₂ / Pd/C / diethyl ether / atmospheric pressure

With sulfuric acid; hydrogen; nitric acid; acetic acid; palladium on activated charcoal; In diethyl ether; 1: Fischer esterification;
DOI:10.1055/s-2005-869900