Technology Process of C43H45F3N4O8
There total 6 articles about C43H45F3N4O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
calcium sulfate; scandium tris(trifluoromethanesulfonate);
In
1,2-dichloro-ethane;
at -30 - 30 ℃;
for 10h;
DOI:10.1002/anie.201308016
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
1.2: 0.33 h / -78 °C
1.3: -78 - 20 °C
2.1: boron tribromide / dichloromethane / 6 h / -78 - 0 °C
3.1: trimethylsilyl trifluoromethanesulfonate; calcium sulfate / 1,2-dichloro-ethane / 3 h / -30 - -10 °C / Inert atmosphere
4.1: scandium tris(trifluoromethanesulfonate); calcium sulfate / 1,2-dichloro-ethane / 10 h / -30 - 30 °C
With
calcium sulfate; trimethylsilyl trifluoromethanesulfonate; boron tribromide; scandium tris(trifluoromethanesulfonate); lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/anie.201308016
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trimethylsilyl trifluoromethanesulfonate; calcium sulfate / 1,2-dichloro-ethane / 7 h / -30 - 10 °C / Inert atmosphere
2: magnesium iodide diethyletherate / diethyl ether; tetrahydrofuran / 5 h / 0 - 50 °C
3: scandium tris(trifluoromethanesulfonate); calcium sulfate / 1,2-dichloro-ethane / 10 h / -30 - 30 °C
With
calcium sulfate; magnesium iodide diethyletherate; trimethylsilyl trifluoromethanesulfonate; scandium tris(trifluoromethanesulfonate);
In
tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1002/anie.201308016