Technology Process of C24H19F4N3O2S
There total 6 articles about C24H19F4N3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate;
In
N,N-dimethyl-formamide;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tricyclohexylphosphine; potassium phosphate / palladium diacetate / toluene; water / 5 h / 100 °C
2.1: sodium hydroxide; water / methanol / 20 °C
2.2: pH 4 - 5
3.1: triethylamine; diphenylphosphoranyl azide / 7 h / Reflux
4.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C
4.2: 20 °C
5.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C
6.1: sodium carbonate / N,N-dimethyl-formamide / 20 °C
With
potassium phosphate; diphenylphosphoranyl azide; water; sodium hydride; sodium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide; tricyclohexylphosphine;
palladium diacetate;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydroxide; water / methanol / 20 °C
1.2: pH 4 - 5
2.1: triethylamine; diphenylphosphoranyl azide / 7 h / Reflux
3.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C
3.2: 20 °C
4.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C
5.1: sodium carbonate / N,N-dimethyl-formamide / 20 °C
With
diphenylphosphoranyl azide; water; sodium hydride; sodium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;