N-[4-methoxy-1-(4-methoxy-phenyl)-but-2-enyl]-N-phenyl-hydroxylamine

Base Information

• Chemical Name: N-[4-methoxy-1-(4-methoxy-phenyl)-but-2-enyl]-N-phenyl-hydroxylamine
• CAS No.: 390423-33-3
• Molecular Formula: C₁₈H₂₁NO₃
• Molecular Weight: 299.37
• Mol file: 390423-33-3.mol

Synonyms:N-[4-methoxy-1-(4-methoxy-phenyl)-but-2-enyl]-N-phenyl-hydroxylamine

Chemical Property of N-[4-methoxy-1-(4-methoxy-phenyl)-but-2-enyl]-N-phenyl-hydroxylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[4-methoxy-1-(4-methoxy-phenyl)-but-2-enyl]-N-phenyl-hydroxylamine

There total 1 articles about N-[4-methoxy-1-(4-methoxy-phenyl)-but-2-enyl]-N-phenyl-hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-methoxydiphenylnitrone (3585-93-1,85225-54-3,87289-90-5) + hex-1-yne (693-02-7) → N-[4-methoxy-1-(4-methoxy-phenyl)-but-2-enyl]-N-phenyl-hydroxylamine (390423-33-3)

Guidance literature:

hex-1-yne; With Schwartz's reagent; In dichloromethane; at 20 ℃; for 1h;

With diethylzinc; In dichloromethane; toluene; at -65 ℃; for 0.25h;

p-methoxydiphenylnitrone; In dichloromethane; toluene; at 0 ℃; for 6h; Further stages.;

DOI:10.1039/b104427n

Reference yield:

N-[4-methoxy-1-(4-methoxy-phenyl)-but-2-enyl]-N-phenyl-hydroxylamine (390423-33-3) → O-[1-methoxymethyl-3-(4-methoxy-phenyl)-allyl]-N-phenyl-hydroxylamine

Guidance literature:

With air; at 20 ℃; for 24h;

DOI:10.1039/b104427n

Reference yield:

N-[4-methoxy-1-(4-methoxy-phenyl)-but-2-enyl]-N-phenyl-hydroxylamine (390423-33-3) → (E)-1-Methoxy-4-phenyl-but-3-en-2-ol

Guidance literature:

Multi-step reaction with 2 steps

1: air / 24 h / 20 °C

2: 100 percent / Zn; AcOH / methanol / 2 h / 40 °C

With air; acetic acid; zinc; In methanol;

DOI:10.1039/b104427n

upstream raw materials:

p-methoxydiphenylnitrone

hex-1-yne