(2S,3R)-2-(N,N'-bis(benzyloxycarbonyl)hydrazino)-3-(tert-butyldimethylsilyloxy)dodecanol

Base Information

Chemical Name:(2S,3R)-2-(N,N'-bis(benzyloxycarbonyl)hydrazino)-3-(tert-butyldimethylsilyloxy)dodecanol
CAS No.:1235561-83-7
Molecular Formula:C₃₄H₅₄N₂O₆Si
Molecular Weight:614.898
Hs Code.:

Synonyms:(2S,3R)-2-(N,N'-bis(benzyloxycarbonyl)hydrazino)-3-(tert-butyldimethylsilyloxy)dodecanol

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Chemical Property of (2S,3R)-2-(N,N'-bis(benzyloxycarbonyl)hydrazino)-3-(tert-butyldimethylsilyloxy)dodecanol

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Technology Process of (2S,3R)-2-(N,N'-bis(benzyloxycarbonyl)hydrazino)-3-(tert-butyldimethylsilyloxy)dodecanol

There total 1 articles about (2S,3R)-2-(N,N'-bis(benzyloxycarbonyl)hydrazino)-3-(tert-butyldimethylsilyloxy)dodecanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 913655-51-3
(R)-3-(tert-butyldimethylsilyloxy)dodecanal

: 2449-05-0
dibenzyl azodicarboxylate

: 1235561-83-7
(2S,3R)-2-(N,N'-bis(benzyloxycarbonyl)hydrazino)-3-(tert-butyldimethylsilyloxy)dodecanol

Guidance literature:: (R)-3-(tert-butyldimethylsilyloxy)dodecanal; dibenzyl azodicarboxylate; With L-proline; In acetonitrile; at 20 ℃; for 2h; Inert atmosphere;

With sodium tetrahydroborate; In ethanol; acetonitrile; at 0 ℃; for 0.0833333h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo1003899