C₃₃H₃₄N₂O₇S

Base Information

Chemical Name:C₃₃H₃₄N₂O₇S
CAS No.:1352230-46-6
Molecular Formula:C₃₃H₃₄N₂O₇S
Molecular Weight:602.708
Hs Code.:

C<sub>33</sub>H<sub>34</sub>N<sub>2</sub>O<sub>7</sub>S

Synonyms:C₃₃H₃₄N₂O₇S

Suppliers and Price of C₃₃H₃₄N₂O₇S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₃₄N₂O₇S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₃₄N₂O₇S

There total 19 articles about C₃₃H₃₄N₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1352230-39-7
C₁₂H₁₆N₂O₅S

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1352230-46-6
C₃₃H₃₄N₂O₇S

Guidance literature:: With pyridine; at 0 - 20 ℃; for 6.5h;

Reference yield:

: 3-O-(naphthalene-2-ylmethyl)-1,2;5,6-0-di(isopropylidene)-α-D-allofuranose

: 1352230-46-6
C₃₃H₃₄N₂O₇S

Guidance literature:: Multi-step reaction with 15 steps

1.1: water; acetic acid / 16 h / 20 °C

2.1: sodium periodate / 1,4-dioxane; water / 1.67 h

3.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

4.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

5.2: 1 h / -78 - 20 °C

6.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

6.2: 3 h / -78 °C

6.3: 20 °C

7.1: sulfuric acid / 2 h / 20 °C

8.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

8.2: 0 - 60 °C

9.1: potassium carbonate / methanol / 96 h / 20 °C

9.2: 12 h / 0 °C

10.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C

10.2: 1.5 h

11.1: pyridine / 5.5 h / 0 - 20 °C

12.1: potassium thioacetate / N,N-dimethyl-formamide / 4 h / 20 °C

12.2: 12 h

13.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 3.5 h

14.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h

15.1: pyridine / 6.5 h / 0 - 20 °C

With pyridine; sodium periodate; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; water; potassium carbonate; acetic acid; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; potassium thioacetate; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1057385-93-9
(3aR,5S,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxole-5-carbaldehyde

: 1352230-46-6
C₃₃H₃₄N₂O₇S

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

2.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

3.2: 1 h / -78 - 20 °C

4.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

4.2: 3 h / -78 °C

4.3: 20 °C

5.1: sulfuric acid / 2 h / 20 °C

6.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

6.2: 0 - 60 °C

7.1: potassium carbonate / methanol / 96 h / 20 °C

7.2: 12 h / 0 °C

8.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C

8.2: 1.5 h

9.1: pyridine / 5.5 h / 0 - 20 °C

10.1: potassium thioacetate / N,N-dimethyl-formamide / 4 h / 20 °C

10.2: 12 h

11.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 3.5 h

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h

13.1: pyridine / 6.5 h / 0 - 20 °C

With pyridine; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; water; potassium carbonate; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; potassium thioacetate; sulfuric acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;