N-[(1S)-1-({2-[(2-{3-[(2-{[2-(3-{[2-({2-[(2S)-2-{[(tert-butoxy)carbonyl]amino}-3-phenylpropanamido]ethyl}disulfanyl)ethyl]carbamoyl}propanamido)ethyl]disulfanyl}ethyl)carbamoyl]propanamido}ethyl)disulfanyl]ethyl}carbamoyl)-2-phenylethyl]carbamic acid tert-butyl ester

Base Information

• Chemical Name: N-[(1S)-1-({2-[(2-{3-[(2-{[2-(3-{[2-({2-[(2S)-2-{[(tert-butoxy)carbonyl]amino}-3-phenylpropanamido]ethyl}disulfanyl)ethyl]carbamoyl}propanamido)ethyl]disulfanyl}ethyl)carbamoyl]propanamido}ethyl)disulfanyl]ethyl}carbamoyl)-2-phenylethyl]carbamic acid tert-butyl ester
• CAS No.: 1313492-40-8
• Molecular Formula: C₄₈H₇₄N₈O₁₀S₆
• Molecular Weight: 1115.56

Synonyms:N-[(1S)-1-({2-[(2-{3-[(2-{[2-(3-{[2-({2-[(2S)-2-{[(tert-butoxy)carbonyl]amino}-3-phenylpropanamido]ethyl}disulfanyl)ethyl]carbamoyl}propanamido)ethyl]disulfanyl}ethyl)carbamoyl]propanamido}ethyl)disulfanyl]ethyl}carbamoyl)-2-phenylethyl]carbamic acid tert-butyl ester

Chemical Property of N-[(1S)-1-({2-[(2-{3-[(2-{[2-(3-{[2-({2-[(2S)-2-{[(tert-butoxy)carbonyl]amino}-3-phenylpropanamido]ethyl}disulfanyl)ethyl]carbamoyl}propanamido)ethyl]disulfanyl}ethyl)carbamoyl]propanamido}ethyl)disulfanyl]ethyl}carbamoyl)-2-phenylethyl]carbamic acid tert-butyl ester

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Technology Process of N-[(1S)-1-({2-[(2-{3-[(2-{[2-(3-{[2-({2-[(2S)-2-{[(tert-butoxy)carbonyl]amino}-3-phenylpropanamido]ethyl}disulfanyl)ethyl]carbamoyl}propanamido)ethyl]disulfanyl}ethyl)carbamoyl]propanamido}ethyl)disulfanyl]ethyl}carbamoyl)-2-phenylethyl]carbamic acid tert-butyl ester

There total 3 articles about N-[(1S)-1-({2-[(2-{3-[(2-{[2-(3-{[2-({2-[(2S)-2-{[(tert-butoxy)carbonyl]amino}-3-phenylpropanamido]ethyl}disulfanyl)ethyl]carbamoyl}propanamido)ethyl]disulfanyl}ethyl)carbamoyl]propanamido}ethyl)disulfanyl]ethyl}carbamoyl)-2-phenylethyl]carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

DSCDI (191794-44-2) + C18H29N3O3S2 (217655-65-7) → N-[(1S)-1-({2-[(2-{3-[(2-{[2-(3-{[2-({2-[(2S)-2-{[(tert-butoxy)carbonyl]amino}-3-phenylpropanamido]ethyl}disulfanyl)ethyl]carbamoyl}propanamido)ethyl]disulfanyl}ethyl)carbamoyl]propanamido}ethyl)disulfanyl]ethyl}carbamoyl)-2-phenylethyl]carbamic acid tert-butyl ester (1313492-40-8)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.bmc.2011.04.022

Reference yield:

Boc-Phe-ONSu (3674-06-4) → N-[(1S)-1-({2-[(2-{3-[(2-{[2-(3-{[2-({2-[(2S)-2-{[(tert-butoxy)carbonyl]amino}-3-phenylpropanamido]ethyl}disulfanyl)ethyl]carbamoyl}propanamido)ethyl]disulfanyl}ethyl)carbamoyl]propanamido}ethyl)disulfanyl]ethyl}carbamoyl)-2-phenylethyl]carbamic acid tert-butyl ester (1313492-40-8)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / methanol; N,N-dimethyl-formamide

2: N,N-dimethyl-formamide / 20 °C

With triethylamine; In methanol; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2011.04.022

Reference yield:

N,N'-(3,4-dithia-hexanediyl)-bis-succinamic acid (108725-86-6) → N-[(1S)-1-({2-[(2-{3-[(2-{[2-(3-{[2-({2-[(2S)-2-{[(tert-butoxy)carbonyl]amino}-3-phenylpropanamido]ethyl}disulfanyl)ethyl]carbamoyl}propanamido)ethyl]disulfanyl}ethyl)carbamoyl]propanamido}ethyl)disulfanyl]ethyl}carbamoyl)-2-phenylethyl]carbamic acid tert-butyl ester (1313492-40-8)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide

2: N,N-dimethyl-formamide / 20 °C

In N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2011.04.022

upstream raw materials:

DSCDI

C₁₈H₂₉N₃O₃S₂

N,N'-(3,4-dithia-hexanediyl)-bis-succinamic acid

Boc-Phe-ONSu

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