C₄₉H₆₄N₂O₁₁Si

Base Information

Chemical Name:C₄₉H₆₄N₂O₁₁Si
CAS No.:1404078-85-8
Molecular Formula:C₄₉H₆₄N₂O₁₁Si
Molecular Weight:885.139
Hs Code.:

C<sub>49</sub>H<sub>64</sub>N<sub>2</sub>O<sub>11</sub>Si

Synonyms:C₄₉H₆₄N₂O₁₁Si

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Chemical Property of C₄₉H₆₄N₂O₁₁Si

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Technology Process of C₄₉H₆₄N₂O₁₁Si

There total 15 articles about C₄₉H₆₄N₂O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1404078-84-7
2-{(2S,3R,4R)-2-(tert-butyldimethylsilyloxy)-4-[(4-methoxybenzyl)oxy]-3-methylhexyl}-4-[(E)-2-iodovinyl]oxazole

: 62-23-7
4-nitro-benzoic acid

: 1404078-85-8
C₄₉H₆₄N₂O₁₁Si

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 0.5h;
DOI:10.1039/c2ob26256h

Reference yield:

: 627511-81-3
(2S,3R)-3-(4-methoxybenzyloxy)-2-methylpentanal

: 1404078-85-8
C₄₉H₆₄N₂O₁₁Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: titanium tetrachloride / dichloromethane / 0.33 h / -50 °C

1.2: 2 h / -40 °C

1.3: 2 h / -78 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 3 h / -78 - 20 °C

3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 - 20 °C

4.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; benzotriazol-1-ol / dichloromethane / 2 h / 20 °C

4.2: 72 h / 20 °C

5.1: diethylamino-sulfur trifluoride / dichloromethane / 2 h / -78 °C

6.1: copper(ll) bromide; hexamethylenetetramine; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2 h / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.75 h / -78 °C

8.1: potassium carbonate / methanol / 0 - 20 °C

9.1: Schwartz's reagent / tetrahydrofuran / 1 h / 0 °C

9.2: 0.67 h / -78 °C / Darkness

10.1: tert.-butyl lithium / pentane; diethyl ether / 1 h / -78 °C / Inert atmosphere

10.2: 0.25 h / -78 °C

10.3: 3 h / -78 °C

11.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 0.5 h / 0 - 20 °C

With 2,6-dimethylpyridine; Schwartz's reagent; diethylamino-sulfur trifluoride; hexamethylenetetramine; dihydrogen peroxide; tert.-butyl lithium; titanium tetrachloride; diisobutylaluminium hydride; potassium carbonate; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; triphenylphosphine; copper(ll) bromide; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; pentane;
DOI:10.1039/c2ob26256h

Reference yield:

: C₂₂H₃₃NO₄S₂

: 1404078-85-8
C₄₉H₆₄N₂O₁₁Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 3 h / -78 - 20 °C

2.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; benzotriazol-1-ol / dichloromethane / 2 h / 20 °C

3.2: 72 h / 20 °C

4.1: diethylamino-sulfur trifluoride / dichloromethane / 2 h / -78 °C

5.1: copper(ll) bromide; hexamethylenetetramine; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2 h / 20 °C

6.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.75 h / -78 °C

7.1: potassium carbonate / methanol / 0 - 20 °C

8.1: Schwartz's reagent / tetrahydrofuran / 1 h / 0 °C

8.2: 0.67 h / -78 °C / Darkness

9.1: tert.-butyl lithium / pentane; diethyl ether / 1 h / -78 °C / Inert atmosphere

9.2: 0.25 h / -78 °C

9.3: 3 h / -78 °C

10.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 0.5 h / 0 - 20 °C

With 2,6-dimethylpyridine; Schwartz's reagent; diethylamino-sulfur trifluoride; hexamethylenetetramine; dihydrogen peroxide; tert.-butyl lithium; diisobutylaluminium hydride; potassium carbonate; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; triphenylphosphine; copper(ll) bromide; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; pentane;
DOI:10.1039/c2ob26256h