1-(2-amino-1-phenylethyl)-3-oxo-1,3-dihydroisobenzofuran-1ylphosphonic acid

Base Information

Chemical Name:1-(2-amino-1-phenylethyl)-3-oxo-1,3-dihydroisobenzofuran-1ylphosphonic acid
CAS No.:134435-12-4
Molecular Formula:C₁₆H₁₆NO₅P
Molecular Weight:333.28
Hs Code.:

Synonyms:1-(2-amino-1-phenylethyl)-3-oxo-1,3-dihydroisobenzofuran-1ylphosphonic acid

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Chemical Property of 1-(2-amino-1-phenylethyl)-3-oxo-1,3-dihydroisobenzofuran-1ylphosphonic acid

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Technology Process of 1-(2-amino-1-phenylethyl)-3-oxo-1,3-dihydroisobenzofuran-1ylphosphonic acid

There total 3 articles about 1-(2-amino-1-phenylethyl)-3-oxo-1,3-dihydroisobenzofuran-1ylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 134435-11-3
dimethyl 1-(2-nitro-1-phenylethyl)-3-oxo-1,3-dihydroisobenzofuran-1ylphosphonate

: 134435-12-4
1-(2-amino-1-phenylethyl)-3-oxo-1,3-dihydroisobenzofuran-1ylphosphonic acid

Guidance literature:: With hydrogen; nickel; In methanol; at 20 ℃; for 4h; under 3040 Torr;

Reference yield:

: 61260-15-9
dimethyl (3-oxo-1,3-dihydroisobenzofuran-1-yl)phosphonate

: 134435-12-4
1-(2-amino-1-phenylethyl)-3-oxo-1,3-dihydroisobenzofuran-1ylphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Na / methanol / 1 h / 20 °C

2: 78 percent / H₂ / Raney nickel / methanol / 4 h / 20 °C / 3040 Torr

With hydrogen; sodium; nickel; In methanol;

Reference yield:

: 102-96-5
(2-nitroethenyl)benzene

: 134435-12-4
1-(2-amino-1-phenylethyl)-3-oxo-1,3-dihydroisobenzofuran-1ylphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Na / methanol / 1 h / 20 °C

2: 78 percent / H₂ / Raney nickel / methanol / 4 h / 20 °C / 3040 Torr

With hydrogen; sodium; nickel; In methanol;